广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
21期
112-114
,共3页
王慧娟%周惠%谷灵灵%刘美凤
王慧娟%週惠%穀靈靈%劉美鳳
왕혜연%주혜%곡령령%류미봉
生北马兜铃%蜜炙北马兜铃%挥发油%GC-MS
生北馬兜鈴%蜜炙北馬兜鈴%揮髮油%GC-MS
생북마두령%밀자북마두령%휘발유%GC-MS
crude Aristolochia contorta%honey processed Aristolochia contorta%violate oil%GC-MS
以环己烷为溶剂,用水蒸气蒸馏法分别来提取生北马兜铃和蜜炙北马兜铃的挥发油,用气-质联用(GC-MS)技术对挥发油的成分进行鉴定,同时以总离子流图为依据,用归一化法计算各成分的相对含量。从生北马兜铃的挥发油中鉴定出57个化合物,主要成分为:4-蔻烯(9.74%),β-石竹烯(9.65%);蜜炙北马兜铃的挥发油中鉴定出28个化合物,主要成分为:邻苯二甲酸二丁酯(18.4%)。北马兜铃蜜炙前后的挥发油中共有成分7个,生成新化合物21个。
以環己烷為溶劑,用水蒸氣蒸餾法分彆來提取生北馬兜鈴和蜜炙北馬兜鈴的揮髮油,用氣-質聯用(GC-MS)技術對揮髮油的成分進行鑒定,同時以總離子流圖為依據,用歸一化法計算各成分的相對含量。從生北馬兜鈴的揮髮油中鑒定齣57箇化閤物,主要成分為:4-蔻烯(9.74%),β-石竹烯(9.65%);蜜炙北馬兜鈴的揮髮油中鑒定齣28箇化閤物,主要成分為:鄰苯二甲痠二丁酯(18.4%)。北馬兜鈴蜜炙前後的揮髮油中共有成分7箇,生成新化閤物21箇。
이배기완위용제,용수증기증류법분별래제취생북마두령화밀자북마두령적휘발유,용기-질련용(GC-MS)기술대휘발유적성분진행감정,동시이총리자류도위의거,용귀일화법계산각성분적상대함량。종생북마두령적휘발유중감정출57개화합물,주요성분위:4-구희(9.74%),β-석죽희(9.65%);밀자북마두령적휘발유중감정출28개화합물,주요성분위:린분이갑산이정지(18.4%)。북마두령밀자전후적휘발유중공유성분7개,생성신화합물21개。
Steam distillation was used to extract the violate oil in crude aristolochia contorta and honey processed aristolochia contorta by using the cyclohexane as solvent.The compounds of volatile oil from the aristolochia were identified by GC-MS technology,the amount of compounds was determined by area normalization method.Fifty-seven compounds were separated and identified from crude Aristolochia contorta,main compounds were 4-Thujene(9.74%) and β-Caryophyllene(9.65%).While twenty-eight compounds were identified from honey processed Aristolochia contorta,main compound was dibutyl phthalate(18.4%).There were 7 mutual components in crude Aristolochia contorta and honey processed Aristolochia contorta,21 new components appeared after honey processed.