广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
22期
51-52,80
,共3页
CdS%合成%微波
CdS%閤成%微波
CdS%합성%미파
CdS%preparation%microwave
利用微波水热技术合成CdS半导体纳米晶体,可以克服有机合成方法毒性大,成本高等问题,通过XRD、TEM表征,产物CdS半导体纳米晶体具有立方晶相,纯度较高。通过紫外吸收光谱和荧光光谱分析,发现该方法制备出的半导体CdS纳米晶体具有良好的光致发光性质,证明水相同样适合高质量CdS半导体纳米晶体的生长。
利用微波水熱技術閤成CdS半導體納米晶體,可以剋服有機閤成方法毒性大,成本高等問題,通過XRD、TEM錶徵,產物CdS半導體納米晶體具有立方晶相,純度較高。通過紫外吸收光譜和熒光光譜分析,髮現該方法製備齣的半導體CdS納米晶體具有良好的光緻髮光性質,證明水相同樣適閤高質量CdS半導體納米晶體的生長。
이용미파수열기술합성CdS반도체납미정체,가이극복유궤합성방법독성대,성본고등문제,통과XRD、TEM표정,산물CdS반도체납미정체구유립방정상,순도교고。통과자외흡수광보화형광광보분석,발현해방법제비출적반도체CdS납미정체구유량호적광치발광성질,증명수상동양괄합고질량CdS반도체납미정체적생장。
CdS semiconductor nanocrystals(NCs) were synthesized by microwave-hydrothermal method in water solution.In comparison,with the synthesis of NCs in organic solvents,the growth surroundings of aqueous NCs were more poisonous and costly.The XRD and TEM provided direct evidence for a cubic zinc blende structure of bulk CdS crystal.Moreover,the CdS NCs had excellent photoluminescence properties by the characterizations of absorption spectra and luminescence spectra.This method proved that CdS NCs suited to grow in aqueous condition.