中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
10期
1765-1767
,共3页
舒乐冲剂%薄层色谱鉴别%含量测定
舒樂遲劑%薄層色譜鑒彆%含量測定
서악충제%박층색보감별%함량측정
Shulegranules%TLC%Contentdetermination
目的：：建立舒乐冲剂的质量标准。方法：采用TLC 对舒乐冲剂中当归、三七、路路通和益母草进行定性鉴别,采用HPLC法对舒乐冲剂中三七皂苷R1、人参皂苷Rg1含量进行测定。结果：定性鉴别斑点清晰,分离度好,专属性强；三七皂苷R1和人参皂苷Rg1两种主成分含量分别为0.1666,0.6818 mg·g-1。结论：建立的舒乐冲剂TLC和 HPLC-UV含量测定方法简便、准确、重复性好,可作为舒乐冲剂质量控制的方法。
目的：：建立舒樂遲劑的質量標準。方法：採用TLC 對舒樂遲劑中噹歸、三七、路路通和益母草進行定性鑒彆,採用HPLC法對舒樂遲劑中三七皂苷R1、人參皂苷Rg1含量進行測定。結果：定性鑒彆斑點清晰,分離度好,專屬性彊；三七皂苷R1和人參皂苷Rg1兩種主成分含量分彆為0.1666,0.6818 mg·g-1。結論：建立的舒樂遲劑TLC和 HPLC-UV含量測定方法簡便、準確、重複性好,可作為舒樂遲劑質量控製的方法。
목적：：건립서악충제적질량표준。방법：채용TLC 대서악충제중당귀、삼칠、로로통화익모초진행정성감별,채용HPLC법대서악충제중삼칠조감R1、인삼조감Rg1함량진행측정。결과：정성감별반점청석,분리도호,전속성강；삼칠조감R1화인삼조감Rg1량충주성분함량분별위0.1666,0.6818 mg·g-1。결론：건립적서악충제TLC화 HPLC-UV함량측정방법간편、준학、중복성호,가작위서악충제질량공제적방법。
Objective:To establish the quality standard for Shule granules. Methods:By TLC, Angelic asinensis, Panax pseudog-inseng, Fructus liquidam-baris and Leonurus in Shule granules were qualitatively identified;and contents of notoginsenoside R1 and gin-senosides Rg1 in Shule granules were quantitatively determined by HPLC. Results: In the qualitative identification, the clear spots showed good resolution and specificity. The content of notoginsenoside R1 and ginsenosides Rg1 , two main ingredients in Shule gran-ules, was 0. 166 6 and 0. 681 8 mg·g-1 , respectively. Conclusion:The TLC and HPLC-UV determination method is simple, accu-rate and reproducible, and can be used as the quality control method for Shule granules.
