科技创新导报
科技創新導報
과기창신도보
SCIENCE AND TECHNOLOGY CONSULTING HERALD
2014年
11期
102-103
,共2页
苯并(a)芘%Cleanert BAP固相萃取柱%芝麻油%反相高效液相色谱法
苯併(a)芘%Cleanert BAP固相萃取柱%芝痳油%反相高效液相色譜法
분병(a)비%Cleanert BAP고상췌취주%지마유%반상고효액상색보법
benzo(a)pyrene%Cleanert BAP Solid phase extraction column%sesame oil%reversed phase high performance liquid chromatographic method
该文采用反相高效液相色谱法测定芝麻油中的苯并(a)芘，分别用Cleanert BAP固相萃取柱和自制固相萃取柱净化,荧光检测器进行检测。结果表明，使用Cleanert BAP固相萃取柱的重现性优于自制的固相萃取柱，回收率在91%～100.5%之间，RSD为3.1%，且操作简便，结果准确可靠。
該文採用反相高效液相色譜法測定芝痳油中的苯併(a)芘，分彆用Cleanert BAP固相萃取柱和自製固相萃取柱淨化,熒光檢測器進行檢測。結果錶明，使用Cleanert BAP固相萃取柱的重現性優于自製的固相萃取柱，迴收率在91%～100.5%之間，RSD為3.1%，且操作簡便，結果準確可靠。
해문채용반상고효액상색보법측정지마유중적분병(a)비，분별용Cleanert BAP고상췌취주화자제고상췌취주정화,형광검측기진행검측。결과표명，사용Cleanert BAP고상췌취주적중현성우우자제적고상췌취주，회수솔재91%～100.5%지간，RSD위3.1%，차조작간편，결과준학가고。
Sesame oil benzo(a)pyrene is determinated with reversed phase high performance liquid chromatographic method, purged by Cleanert BAP Solid phase extraction column and Self-control Solid phase extraction column,detected by the fluorescence detector.The result shows that the reproducibility by Cleanert BAP Solid phase extraction column is better than by Self-control Solid phase extraction column,the tecoverie is range from 91% to 100.5%,the RSD is 3.1%.This is a good method that the operation is convenient and the result is accurate and reliable.
