CAJ | 학술논문

　　目的采用合理的样品前处理方法改善食品包装材料中2,6二叔丁基苯酚(BHT)的GC-MS分析效果。方法正己烷超声辅助萃取塑料包装材料碎片后,将提取液在?10℃条件下放置2 d,萃取液离心,将上清液旋转蒸发浓缩,进行GC-MS分析。结果 GC-MS分析总离子流图中BHT峰形干净、杂质峰值明显减少。结论该前处理方法能明显改善GC-MS分析效果。
　　목적채용합리적양품전처리방법개선식품포장재료중2,6이숙정기분분(BHT)적GC-MS분석효과。방법정기완초성보조췌취소료포장재료쇄편후,장제취액재?10℃조건하방치2 d,췌취액리심,장상청액선전증발농축,진행GC-MS분석。결과 GC-MS분석총리자류도중BHT봉형간정、잡질봉치명현감소。결론해전처리방법능명현개선GC-MS분석효과。
Objective To improve the GC-MS study of 2,6-butylated hydroxytoluene (BHT) by reasonable pretreatment of sample extracted from food plastic packaging materials. Methods Samples were extracted with hexane under ultrasound assisted extraction, stored for 2 d under?10℃, and analyzed by GC-MS after centrifu-gation and concentration. Results Total ion chromatograms of BHT GC-MS peak was clean, and impurity peak was significantly reduced. Conclusion The pre-treatment method could significantly improve the GC-MS study of 2,6-butylated hydroxytoluene (BHT).