华南师范大学学报(自然科学版)
華南師範大學學報(自然科學版)
화남사범대학학보(자연과학판)
JOURNAL OF SOUTH CHINA NORMAL UNIVERSITY (NATURAL SCIENCE EDITION)
2014年
3期
87-93
,共7页
尾矿%回收%白钨矿%浮选%工艺
尾礦%迴收%白鎢礦%浮選%工藝
미광%회수%백오광%부선%공예
tailings%recovering%scheelite%floatation%technology process
研究采用再磨-浮选工艺对南方某老尾库尾矿(含 WO30.19%)中的钨进行回收.以 NaOH 为调整剂、Na2 SiO3为抑制剂、氧化石蜡皂733为捕收剂,当-0.074 mm 占83.52%的磨矿细度下,钨粗选试验最佳条件为 NaOH 用量为2000 g/ t,Na2 SiO3用量为2000 g/ t,捕收剂733用量为100 g/ t.通过一次粗选、二次扫选和三次精选流程,获得钨粗精矿含 WO33.26%,回收率为70.48%.红外光谱测定结果表明,捕收剂733对白钨矿的捕收作用以表面化学吸附和键合为主.
研究採用再磨-浮選工藝對南方某老尾庫尾礦(含 WO30.19%)中的鎢進行迴收.以 NaOH 為調整劑、Na2 SiO3為抑製劑、氧化石蠟皂733為捕收劑,噹-0.074 mm 佔83.52%的磨礦細度下,鎢粗選試驗最佳條件為 NaOH 用量為2000 g/ t,Na2 SiO3用量為2000 g/ t,捕收劑733用量為100 g/ t.通過一次粗選、二次掃選和三次精選流程,穫得鎢粗精礦含 WO33.26%,迴收率為70.48%.紅外光譜測定結果錶明,捕收劑733對白鎢礦的捕收作用以錶麵化學吸附和鍵閤為主.
연구채용재마-부선공예대남방모로미고미광(함 WO30.19%)중적오진행회수.이 NaOH 위조정제、Na2 SiO3위억제제、양화석사조733위포수제,당-0.074 mm 점83.52%적마광세도하,오조선시험최가조건위 NaOH 용량위2000 g/ t,Na2 SiO3용량위2000 g/ t,포수제733용량위100 g/ t.통과일차조선、이차소선화삼차정선류정,획득오조정광함 WO33.26%,회수솔위70.48%.홍외광보측정결과표명,포수제733대백오광적포수작용이표면화학흡부화건합위주.
The process of recovery of tungsten by regrinding-flotation from an old ore tailing contained 0. 19% WO3 in the south is investigated. The results show that satisfactory flotation indexes can be achieved by the process of one stage roughing,two-stage scavenging and three-stage cleaning,with sodium hydroxide as regulator,sodium sili-cate as the depressant and paraffin soap oxidated 733 as the collector. The experiment of tungsten roughing shows that the optimized dosage of NaOH is 2 000 g / t,dosage of sodium silicate is 2 000 g / t,dosage of collector 733 is 100 g / t when the optimum grinding fineness of - 0. 074 mm is 83. 52% . The tungsten concentrate grade and the recovery of WO3 reach 3. 26% and 70. 48% ,respectively. Analysis of IR spectra testified that chemisorption and bonding were the main reaction mechanism of 733 on scheelite.