工程塑料应用
工程塑料應用
공정소료응용
ENGINEERING PLASTICS APPLICATION
2014年
5期
99-104
,共6页
赵文静%麦永懿%张炜%叶纯麟%李志%沈贤婷
趙文靜%麥永懿%張煒%葉純麟%李誌%瀋賢婷
조문정%맥영의%장위%협순린%리지%침현정
多壁碳纳米管%超高分子量聚乙烯%复合纤维%结构%性能
多壁碳納米管%超高分子量聚乙烯%複閤纖維%結構%性能
다벽탄납미관%초고분자량취을희%복합섬유%결구%성능
MWCNT%PE-UHMW%composite fiber%structure%property
对多壁碳纳米管(MWCNT)进行表面有机化改性处理后,采用向纺丝溶剂中滴加纳米粒子悬浮液的混合方式,制备了超高分子量聚乙烯(PE-UHMW)/MWCNT复合纤维。通过紫外分光光度计、扫描电子显微镜、热台偏光显微镜分析了MWCNT在基体中的分散情况,并利用X射线衍射、力学性能测试、差示扫描量热分析、热重分析等测试方法对复合纤维的结构及性能进行了表征分析。结果表明,MWCNT分散良好的复合纤维,其力学性能得到了提升,耐热性和耐蠕变性也得到了不同程度的改善。
對多壁碳納米管(MWCNT)進行錶麵有機化改性處理後,採用嚮紡絲溶劑中滴加納米粒子懸浮液的混閤方式,製備瞭超高分子量聚乙烯(PE-UHMW)/MWCNT複閤纖維。通過紫外分光光度計、掃描電子顯微鏡、熱檯偏光顯微鏡分析瞭MWCNT在基體中的分散情況,併利用X射線衍射、力學性能測試、差示掃描量熱分析、熱重分析等測試方法對複閤纖維的結構及性能進行瞭錶徵分析。結果錶明,MWCNT分散良好的複閤纖維,其力學性能得到瞭提升,耐熱性和耐蠕變性也得到瞭不同程度的改善。
대다벽탄납미관(MWCNT)진행표면유궤화개성처리후,채용향방사용제중적가납미입자현부액적혼합방식,제비료초고분자량취을희(PE-UHMW)/MWCNT복합섬유。통과자외분광광도계、소묘전자현미경、열태편광현미경분석료MWCNT재기체중적분산정황,병이용X사선연사、역학성능측시、차시소묘량열분석、열중분석등측시방법대복합섬유적결구급성능진행료표정분석。결과표명,MWCNT분산량호적복합섬유,기역학성능득도료제승,내열성화내연변성야득도료불동정도적개선。
Multi-walled carbon nano-tubes(MWCNT)/ultra-high molecular weight polyethylene(PE-UHMW) composite fiber was prepared through adding suspension of MWCNT modified with organic reagent drop by drop. The dispersion of MWCNT in polymer matrix was observed and analyzed by ultraviolet spectrophotometer,scanning electron microscopy,thermal platform microscope,and the properties of the composite fiber were characterized using x-ray diffraction,differential scanning caldrimetry, mechanics performance testing,thermogravimetric analysis.The experiment results show that the MWCNT/PE-UHMW fiber is improved in the performances such as mechanical properties,thermal stability and creep resistance.