食品安全质量检测学报
食品安全質量檢測學報
식품안전질량검측학보
FOOD SAFETY AND QUALITY DETECTION TECHNOLOGY
2014年
1期
265-270
,共6页
董海胜%臧鹏%王妮%黄贱英
董海勝%臧鵬%王妮%黃賤英
동해성%장붕%왕니%황천영
电感耦合等离子体发射光谱法%元素%微波消解%茶叶籽
電感耦閤等離子體髮射光譜法%元素%微波消解%茶葉籽
전감우합등리자체발사광보법%원소%미파소해%다협자
inductively coupled plasma atomic emission spectrometry%elements%microwave digestion%tea seeds
目的:对茶叶籽中金属元素进行分析,为茶叶籽综合利用提供参考。方法采用高压密闭微波消解结合电感耦合等离子体发射光谱法对茶叶籽中As、Ca、Cd、Cr、Cu、Fe、K、Mg、Mn、Na、Pb、Se及Zn等元素进行了同时快速定量分析。结果茶叶籽中各元素含量: Mg(1652.23 mg/kg)、Ca(1026.36 mg/kg)、Mn(122.44 mg/kg)、Na(37.77 mg/kg)、Cr(7.58 mg/kg)、Cu(9.11 mg/kg)、Fe(58.17 mg/kg)、Zn(17.59 mg/kg)、K (9191.29 mg/kg)。As、Cd、Pb及Se未检出。方法加标回收率89%~113%。结论此方法满足茶叶籽样品中所述元素的分析要求。茶叶籽中钾、镁及钙含量较高,钠含量相对较低;锰、铁、锌及铬元素含量丰富。
目的:對茶葉籽中金屬元素進行分析,為茶葉籽綜閤利用提供參攷。方法採用高壓密閉微波消解結閤電感耦閤等離子體髮射光譜法對茶葉籽中As、Ca、Cd、Cr、Cu、Fe、K、Mg、Mn、Na、Pb、Se及Zn等元素進行瞭同時快速定量分析。結果茶葉籽中各元素含量: Mg(1652.23 mg/kg)、Ca(1026.36 mg/kg)、Mn(122.44 mg/kg)、Na(37.77 mg/kg)、Cr(7.58 mg/kg)、Cu(9.11 mg/kg)、Fe(58.17 mg/kg)、Zn(17.59 mg/kg)、K (9191.29 mg/kg)。As、Cd、Pb及Se未檢齣。方法加標迴收率89%~113%。結論此方法滿足茶葉籽樣品中所述元素的分析要求。茶葉籽中鉀、鎂及鈣含量較高,鈉含量相對較低;錳、鐵、鋅及鉻元素含量豐富。
목적:대다협자중금속원소진행분석,위다협자종합이용제공삼고。방법채용고압밀폐미파소해결합전감우합등리자체발사광보법대다협자중As、Ca、Cd、Cr、Cu、Fe、K、Mg、Mn、Na、Pb、Se급Zn등원소진행료동시쾌속정량분석。결과다협자중각원소함량: Mg(1652.23 mg/kg)、Ca(1026.36 mg/kg)、Mn(122.44 mg/kg)、Na(37.77 mg/kg)、Cr(7.58 mg/kg)、Cu(9.11 mg/kg)、Fe(58.17 mg/kg)、Zn(17.59 mg/kg)、K (9191.29 mg/kg)。As、Cd、Pb급Se미검출。방법가표회수솔89%~113%。결론차방법만족다협자양품중소술원소적분석요구。다협자중갑、미급개함량교고,납함량상대교저;맹、철、자급락원소함량봉부。
Objective To analyze the etal elements in tea seed, so as to provide a reference for tea seed utilization. Methods Rapid quantitative analysis for elements As, Ca, Cd, Cr, Cu, Fe, K, Mg, Mn, Na, Pb, Se and Zn in tea seeds was carried out by the high-pressure sealed microwave digestion combined with inductively coupled plasma atomic emission spectrometry. Results The content of each element in tea seed were as fol-lowing:Mg (1652.23 mg/kg), Ca (1 026.36 mg/kg), Mn (122.44 mg/kg), Na (37.77 mg/kg) , Cr (7.58 mg/kg), Cu (9.11 mg/kg), Fe (58.17 mg/kg), Zn (17.59 mg/kg) and K (9191.29 mg/kg), while, As, Cd, Pb and Se were not detected. Method recoveries for all the elements used in this research were between 89%and 113%. Con-clusion The method established in this research satisfies the analysis requirements of element in tea seed. Contents of potassium, magnesium and calcium are of high lever in tea seed, while sodium content is relatively low. Tea seed is rich in minor elements such as manganese, iron, zinc and chromium.