CAJ | 학술논문

目的：建立藏药打箭菊的质量标准。方法：采用显微、薄层色谱法建立其鉴别方法；参考2010年版《中国药典》（一部）相关方法测定其水分、总灰分、酸不溶性灰分和浸出物的含量；采用高效液相色谱法测定木犀草素的含量。结果：藏药打箭菊药材的显微、薄层色谱鉴别特征明显，专属性强；打箭菊药材中木犀草素含量为0.036%~0.104%（均值0.078%），水分为9.32%~15.82%（均值13.11%），总灰分为6.65%~8.29%（均值7.45%），酸不溶性灰分为0.23%~0.59%（均值0.42%），浸出物为21.42%~30.15%（均值24.86%）。结论：本文建立的方法操作简单、准确可靠、重复性良好，可用于控制打箭菊药材的质量。
목적：건립장약타전국적질량표준。방법：채용현미、박층색보법건립기감별방법；삼고2010년판《중국약전》（일부）상관방법측정기수분、총회분、산불용성회분화침출물적함량；채용고효액상색보법측정목서초소적함량。결과：장약타전국약재적현미、박층색보감별특정명현，전속성강；타전국약재중목서초소함량위0.036%~0.104%（균치0.078%），수분위9.32%~15.82%（균치13.11%），총회분위6.65%~8.29%（균치7.45%），산불용성회분위0.23%~0.59%（균치0.42%），침출물위21.42%~30.15%（균치24.86%）。결론：본문건립적방법조작간단、준학가고、중복성량호，가용우공제타전국약재적질량。
This study was aimed to establish the quality standard of Pyrethri Tatsienenis Flos. The medical material was identified by the microscopy and the thin layer chromatography ( TLC ) methods . The moisture , total ash , acid-insoluble ash and alcohol-soluble extract were determined according to procedures recorded in the Chi-nese Pharmacopoeia (2010 edition). The content of luteolin was determined by the HPLC method. The results showed a strong characteristic microscopic of Pyrethri Tatsienenis Flos , and its TLC identification had a good resolution with clear spots . The mass fractions of luteolin was 0 . 036%~0 . 104% ( average of 0 . 078%) , moisture was 9 . 32%~15 . 82% ( average of 13 . 11%) , total ash was 6 . 65%~8 . 29% ( average of 7 . 45%) , acid-insoluble ash was 0 . 23%~0 . 59% ( average of 0 . 42%) , and the extraction was 21 . 42%~30 . 15% ( average of 24 . 86%) . It was concluded that this established standard was simple to operate with good stability and reproducibility , which can be used for quality evaluation of Pyrethri Tatsienenis Flos .