世界中医药
世界中醫藥
세계중의약
WORLD CHINESE MEDICINE
2014年
1期
99-100
,共2页
赤小豆%水分%总灰分%水溶性浸出物%杂质含量
赤小豆%水分%總灰分%水溶性浸齣物%雜質含量
적소두%수분%총회분%수용성침출물%잡질함량
Vignae Semen%Moisture%Total ash%Water-soluble extractives%Impurities extract%Content
目的：对不同产地赤小豆药材水分、总灰分、水溶性浸出物和杂质进行测定。方法：按照《中华人民共和国药典》2010年版（一部）附录IX H水分法（烘干法）、附录IX K灰分测定法、附录XA浸出物测定法及附录IX A杂质检查法测定。结果：市售12批赤小豆药材，水分测定结果最高值为13.64％，最低值为10.12％，平均值为11.96％；总灰分测定结果最高值为4.36％，最低值为3.61％，平均值为3.90％，水溶性浸出物测定结果最高值为24.32％，最低值为18.16％，平均值为20.73％；杂质测定结果最高值为1.11％，最低值为0.67％，平均值为0.90％。结论：为进一步完善赤小豆药材质量标准提供依据。
目的：對不同產地赤小豆藥材水分、總灰分、水溶性浸齣物和雜質進行測定。方法：按照《中華人民共和國藥典》2010年版（一部）附錄IX H水分法（烘榦法）、附錄IX K灰分測定法、附錄XA浸齣物測定法及附錄IX A雜質檢查法測定。結果：市售12批赤小豆藥材，水分測定結果最高值為13.64％，最低值為10.12％，平均值為11.96％；總灰分測定結果最高值為4.36％，最低值為3.61％，平均值為3.90％，水溶性浸齣物測定結果最高值為24.32％，最低值為18.16％，平均值為20.73％；雜質測定結果最高值為1.11％，最低值為0.67％，平均值為0.90％。結論：為進一步完善赤小豆藥材質量標準提供依據。
목적：대불동산지적소두약재수분、총회분、수용성침출물화잡질진행측정。방법：안조《중화인민공화국약전》2010년판（일부）부록IX H수분법（홍간법）、부록IX K회분측정법、부록XA침출물측정법급부록IX A잡질검사법측정。결과：시수12비적소두약재，수분측정결과최고치위13.64％，최저치위10.12％，평균치위11.96％；총회분측정결과최고치위4.36％，최저치위3.61％，평균치위3.90％，수용성침출물측정결과최고치위24.32％，최저치위18.16％，평균치위20.73％；잡질측정결과최고치위1.11％，최저치위0.67％，평균치위0.90％。결론：위진일보완선적소두약재질량표준제공의거。
Objective:To determine the contents of the moisture , total ash, water-soluble extract and impurities content of Vignae Semen produced in different areas .Methods:The contents were determined according to water determination method ( drying) in Appendix IX H, ash detection in Appendix IX K , extractives determination in Appendix XA and impurities determination in Appendix IXA of the 2010 edition of “Chinese Pharmacopoeia”.Results:The average moisture content of the 12 batches of commercially available Vignae Semen was 11.96%, and the highest was 13.64%, and the lowest was 10.12%.The total ash average content was 3.90%, and the highest was 4.36%, and the lowest was 3.61%.The average content of water-soluble extract was 20.73%, and the highest was 24.32%and the lowest was18.16%.The average content of impurities was 0.90%, and the highest was 1.11% and the lowest was 0.67%.Conclusion:These data provide the quality standards basis for further establishment and improvement of Vignae Semen .
