粉末冶金材料科学与工程
粉末冶金材料科學與工程
분말야금재료과학여공정
POWDER METALLURGY MATERIALS SCIENCE AND ENGINEERING
2014年
2期
197-204
,共8页
许小龙%倪东惠%张宝霞%谢珩%陈晓莞
許小龍%倪東惠%張寶霞%謝珩%陳曉莞
허소룡%예동혜%장보하%사형%진효완
Ti3SiC2%Cu%复合材料%热稳定性
Ti3SiC2%Cu%複閤材料%熱穩定性
Ti3SiC2%Cu%복합재료%열은정성
Ti3SiC2%Cu%composite%thermal stability
以Cu和表面镀有Cu的Ti3SiC2粉末为原料,采用温压压制成形和复压复烧技术制备一系列Cu-Ti3SiC2复合材料,研究不同烧结温度、Ti3SiC2含量以及复压复烧对材料性能的影响。采用XRD衍射仪、环块式摩擦磨损试验机等测试手段,研究Cu-Ti3SiC2复合材料的物相组成和摩擦磨损行为。研究结果表明:以800℃烧结可制得不含杂质的纯Cu-Ti3SiC2复合材料;而以1000℃烧结制得的复合材料中含有TiC和TiSi2杂质,这些杂质可影响材料的导电性能和减摩能力。复压复烧可使材料的密度、硬度以及导电性能得到不同程度的提高,尤其对于高Ti3SiC2含量的材料,其作用更为明显。
以Cu和錶麵鍍有Cu的Ti3SiC2粉末為原料,採用溫壓壓製成形和複壓複燒技術製備一繫列Cu-Ti3SiC2複閤材料,研究不同燒結溫度、Ti3SiC2含量以及複壓複燒對材料性能的影響。採用XRD衍射儀、環塊式摩抆磨損試驗機等測試手段,研究Cu-Ti3SiC2複閤材料的物相組成和摩抆磨損行為。研究結果錶明:以800℃燒結可製得不含雜質的純Cu-Ti3SiC2複閤材料;而以1000℃燒結製得的複閤材料中含有TiC和TiSi2雜質,這些雜質可影響材料的導電性能和減摩能力。複壓複燒可使材料的密度、硬度以及導電性能得到不同程度的提高,尤其對于高Ti3SiC2含量的材料,其作用更為明顯。
이Cu화표면도유Cu적Ti3SiC2분말위원료,채용온압압제성형화복압복소기술제비일계렬Cu-Ti3SiC2복합재료,연구불동소결온도、Ti3SiC2함량이급복압복소대재료성능적영향。채용XRD연사의、배괴식마찰마손시험궤등측시수단,연구Cu-Ti3SiC2복합재료적물상조성화마찰마손행위。연구결과표명:이800℃소결가제득불함잡질적순Cu-Ti3SiC2복합재료;이이1000℃소결제득적복합재료중함유TiC화TiSi2잡질,저사잡질가영향재료적도전성능화감마능력。복압복소가사재료적밀도、경도이급도전성능득도불동정도적제고,우기대우고Ti3SiC2함량적재료,기작용경위명현。
Using Cu and Cu coated Ti3SiC2 powders as raw materials, a series of Cu-Ti3SiC2 composites were prepared by employing warm compaction forming and double-press double-sinter techniques. Effects of sinter temperature, Ti3SiC2 content and double-press double-sinter on the properties of the prepared composites were studied. Composition and tribological behavior of the Cu-Ti3SiC2 composites were studied by X-ray diffractometer and a block-on-ring tribotester,respectively. Results show that Cu-Ti3SiC2 composites without impurity can be fabricated by sintering at 800℃; however, composites obtained by sintering at 1 000 ℃ contain TiC and TiSi2 impurities, which eventually impose adverse effect on the electrical conductivity and anti-friction ability of the composite. Double-press double-sinter can improve the density, hardness and electrical conductivity of the composites to certain degree, especially for the composite with high Ti3SiC2 content.