CAJ | 학술논문

目的：分析芹菜子的薄层鉴别及水分、灰分、浸出物，为制定芹菜子药材质量标准提供科学依据。方法收集不同批次的芹菜子药材，以芹菜素和木犀草素为指标，采用薄层色谱法建立了薄层鉴别，并按《中国药典》（2010年版一部）中相关规定，对该药材中水分、灰分和浸出物醇浸出物等项目进行测定。结果薄层鉴别结果显示，供试品色谱图中芹菜素和木犀草素的斑点清晰，分离度较好；该药材中水分＜7．5％，总灰分＜15．0％，酸不溶性灰分＜1．5％；采用热浸法，其醇溶性浸出物＞20．0％。结论该组方法简便、准确、重复性好，为建立芹菜子药材质量标准提供了准确可靠的实验依据。
목적：분석근채자적박층감별급수분、회분、침출물，위제정근채자약재질량표준제공과학의거。방법수집불동비차적근채자약재，이근채소화목서초소위지표，채용박층색보법건립료박층감별，병안《중국약전》（2010년판일부）중상관규정，대해약재중수분、회분화침출물순침출물등항목진행측정。결과박층감별결과현시，공시품색보도중근채소화목서초소적반점청석，분리도교호；해약재중수분＜7．5％，총회분＜15．0％，산불용성회분＜1．5％；채용열침법，기순용성침출물＞20．0％。결론해조방법간편、준학、중복성호，위건립근채자약재질량표준제공료준학가고적실험의거。
Objective To develop a scientific method for the quality standards of Celery Seeds .Methods This study collected from different batches of Celery Seeds ,thin-layer chromatography (TLC) identifica-tion method was carried out by using apigenin and luteolin as an indicator ,and determined moisture ,ash , water-soluble extractives ,ethanol-soluble extractives ,addording to The Pharmacopoeia of the PRC .Re-sults The TLC identification method was a specific method with good resolution .The moisture was less than 7 .5% ,total ash was not more than 15 .0% ,acid insoluble ash was not cross over 1 .5% ,ethanol-sol-uble extractives were not less than 20 .0% .Conclusions This method was simple ,accurate and reproduci-ble .The quality standards can provide a reliable experimental basis for Celery Seeds .