CAJ | 학술논문

目的：修订中药材黄药子的质量标准。方法药材粉末的显微鉴别，选用合适的方法测定浸出物，采用高效液相色谱法测定薯蓣皂苷的含量。结果显微鉴别组织特征典型，根据检测结果，暂规定本品水溶性浸出物不得少于15.0%；含薯蓣皂苷应为0.12%～0.29%，薯蓣皂苷在0.01958μg～0.3916μg范围内与峰面积呈良好的线性关系，平均回收率为99.30%（RSD＝0.8%,n＝6）。结论所建立的质量标准方法可靠、准确、专属性强，可有效控制黄药子的质量。
목적：수정중약재황약자적질량표준。방법약재분말적현미감별，선용합괄적방법측정침출물，채용고효액상색보법측정서여조감적함량。결과현미감별조직특정전형，근거검측결과，잠규정본품수용성침출물불득소우15.0%；함서여조감응위0.12%～0.29%，서여조감재0.01958μg～0.3916μg범위내여봉면적정량호적선성관계，평균회수솔위99.30%（RSD＝0.8%,n＝6）。결론소건립적질량표준방법가고、준학、전속성강，가유효공제황약자적질량。
Objective To establish the quality standard for HERBA EUPHORBIAE HELIOSCOPIAE.Methods Microscopic Of Stem cross-section and medicinal powder.Identification of quercetin by TLC,Determination of Quercetin by HPLC. Results The Microscopic identification of organizational characteristics are typical. The characteristic identification by TLC was distinct and highly specific;According to test results,Alcohol-soluble extract temporary provisions shall not be less than 9.0%,Alcohol-soluble extract of not less than 9.0%.Quercetin content of not less than 0.14%,the quantitative evaluation of thymol had the linear range of 0.03916μg~0.7832μg.The average recovery was 99.49% and RSD was RSD=0.74%. Conclusion The method is reliable,accurate and specific,and can be used for the quality control of HERBA EUPHORBIAE HELIOSCOPIAE.