中国陶瓷工业
中國陶瓷工業
중국도자공업
CHINA CERAMIC INDUSTRY
2012年
6期
18-21
,共4页
张玲洁%盛建松%郭兴忠%杨辉
張玲潔%盛建鬆%郭興忠%楊輝
장령길%성건송%곽흥충%양휘
SiC%纳米SiB6%两步烧结%烧结性能力学性能
SiC%納米SiB6%兩步燒結%燒結性能力學性能
SiC%납미SiB6%량보소결%소결성능역학성능
SiC,nano- SiB6%double sintering%sintering performance%mechanical performance
以纳米SiB6颗粒为增强相,YAG为烧结助剂,采用无压液相烧结技术制备了SiC/纳米SiB6复合陶瓷,主要研究两步烧结对复合陶瓷烧结特性和力学性能的影响。研究结果表明,两步烧结对复合陶瓷的烧结性能和力学性能有一定的影响。第一步烧结温度由1850℃升至1900℃,SiC/纳米SiB。复合陶瓷的收缩率、失重率和相对密度增加,抗弯强度和维氏硬度整体下降;而第二步烧结温度由1850℃升高到1900℃,复合陶瓷失重率增加,收缩率和相对密度下降,抗弯强度和维氏硬度均有所提高。
以納米SiB6顆粒為增彊相,YAG為燒結助劑,採用無壓液相燒結技術製備瞭SiC/納米SiB6複閤陶瓷,主要研究兩步燒結對複閤陶瓷燒結特性和力學性能的影響。研究結果錶明,兩步燒結對複閤陶瓷的燒結性能和力學性能有一定的影響。第一步燒結溫度由1850℃升至1900℃,SiC/納米SiB。複閤陶瓷的收縮率、失重率和相對密度增加,抗彎彊度和維氏硬度整體下降;而第二步燒結溫度由1850℃升高到1900℃,複閤陶瓷失重率增加,收縮率和相對密度下降,抗彎彊度和維氏硬度均有所提高。
이납미SiB6과립위증강상,YAG위소결조제,채용무압액상소결기술제비료SiC/납미SiB6복합도자,주요연구량보소결대복합도자소결특성화역학성능적영향。연구결과표명,량보소결대복합도자적소결성능화역학성능유일정적영향。제일보소결온도유1850℃승지1900℃,SiC/납미SiB。복합도자적수축솔、실중솔화상대밀도증가,항만강도화유씨경도정체하강;이제이보소결온도유1850℃승고도1900℃,복합도자실중솔증가,수축솔화상대밀도하강,항만강도화유씨경도균유소제고。
SiC/SiB6 composite ceramics were synthesized by pressureless liquid phase sintering, using SiBe nanoparticles as the reinforcement and YAG as the sintering aid. The effects of two-step sintering on their sintering properties and mechanical performance were studied. Results show, two-step sintering could affect the sintering properties and mechanical performance of the composite ceramics. When the temperature of the first sintering rose from 1850℃ to 1900℃, the contractiveness, mass loss and relative density of SiC/SiBe composite ceramics increased, but the flexural strength and Vickers hardness decreased; when the temperature of the second sintering rose from 1850℃ to 1900℃, the mass loss increased, the contravenes and relative density decreased, but the flexural strength and Vickers hardness were enhanced.