上海电机学院学报
上海電機學院學報
상해전궤학원학보
JOURNAL OF SHANGHAI DIANJI UNIVERSITY
2012年
5期
342-344,350
,共4页
袁艳红%杨党强%柯磊
袁豔紅%楊黨彊%柯磊
원염홍%양당강%가뢰
多壁碳纳米管%缺陷%光致发光
多壁碳納米管%缺陷%光緻髮光
다벽탄납미관%결함%광치발광
multiwalled carbon nanotubes(MWNTs)%defect%photolumineseence
采用化学气相沉积法,在反应温度分别为980℃和1040℃时制备了多壁碳纳米管(MWNTs)样品,并采用扫描电镜和拉曼光谱对样品进行了表征;结果表明,当反应温度为9800C时,制备的碳纳米管结构缺陷更多。使用波长为350nm的光激发2种样品并测量它们的光致发光光谱。发射峰值约在550nm处,反应温度为980℃时制备的碳纳米管的发射光谱的光强较强。
採用化學氣相沉積法,在反應溫度分彆為980℃和1040℃時製備瞭多壁碳納米管(MWNTs)樣品,併採用掃描電鏡和拉曼光譜對樣品進行瞭錶徵;結果錶明,噹反應溫度為9800C時,製備的碳納米管結構缺陷更多。使用波長為350nm的光激髮2種樣品併測量它們的光緻髮光光譜。髮射峰值約在550nm處,反應溫度為980℃時製備的碳納米管的髮射光譜的光彊較彊。
채용화학기상침적법,재반응온도분별위980℃화1040℃시제비료다벽탄납미관(MWNTs)양품,병채용소묘전경화랍만광보대양품진행료표정;결과표명,당반응온도위9800C시,제비적탄납미관결구결함경다。사용파장위350nm적광격발2충양품병측량타문적광치발광광보。발사봉치약재550nm처,반응온도위980℃시제비적탄납미관적발사광보적광강교강。
Muhiwalled carbon nanotubes (MWNTs) were synthesized with chemical vapor deposition(CVD) at 980 ℃ and 1 040 ℃. MWNTs products were characterized with SEM and mi-cro-Raman spectrum. Experimental results show that an additional line due to defects on the outer surface of MWNTs at a reaction temperature 980 ℃. When wavelength of the excitation light was 350 nm, an emission band at about 550 nm was observed in the photoluminescence spectrum for two samples at room temperature. One of them synthesized by chemical vapor deposition at 980 ℃ is intensive.