山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2012年
12期
61-62
,共2页
脱硫液%硫氰酸铵%分析%分光光度法
脫硫液%硫氰痠銨%分析%分光光度法
탈류액%류청산안%분석%분광광도법
desulfurized liquor%ammonium rhodanide%spectrophotometr
用分光光度法测定了焦化脱硫液中硫氰酸铵的含量。通过实验确定反应溶液在460mn有最大吸收。利用分光光度法在该波长下进行比色测定,含量在(O~300)g/L范围内符合比尔定律,其线性回归方程为C=476.19A+0.02(R^2=0.9998)。该方法测定脱硫液中硫氰酸铵含量快速、准确、重现性好、试样无需特殊处理。
用分光光度法測定瞭焦化脫硫液中硫氰痠銨的含量。通過實驗確定反應溶液在460mn有最大吸收。利用分光光度法在該波長下進行比色測定,含量在(O~300)g/L範圍內符閤比爾定律,其線性迴歸方程為C=476.19A+0.02(R^2=0.9998)。該方法測定脫硫液中硫氰痠銨含量快速、準確、重現性好、試樣無需特殊處理。
용분광광도법측정료초화탈류액중류청산안적함량。통과실험학정반응용액재460mn유최대흡수。이용분광광도법재해파장하진행비색측정,함량재(O~300)g/L범위내부합비이정률,기선성회귀방정위C=476.19A+0.02(R^2=0.9998)。해방법측정탈류액중류청산안함량쾌속、준학、중현성호、시양무수특수처리。
In lab ammonium rhodanide in desulfurized liquor was measured by means of spectrophotometr. The substance had maximum absorption at 460nm. When ammonium rhodanide was in the range of (0 - 300) g/L, it was in accord with Beerg law, its linear regression equation was C = 476.19A + 0.02 (R = 0.9998). Rapid, accurate measurement and good repeatability for ammonium rhodanide in desulfurized liquor could be realized by means of the method, no special treatment for sample was made.