世界中医药
世界中醫藥
세계중의약
WORLD CHINESE MEDICINE
2013年
11期
1277-1279
,共3页
杜敏%吴志生%巩颖%史新元%华国栋%乔延江
杜敏%吳誌生%鞏穎%史新元%華國棟%喬延江
두민%오지생%공영%사신원%화국동%교연강
道地山药%近红外漫反射光谱%判别分析法%鉴别
道地山藥%近紅外漫反射光譜%判彆分析法%鑒彆
도지산약%근홍외만반사광보%판별분석법%감별
Genuine Chinese Yam%Near infrared diffuse reflectance spectroscopy%Discriminant analysis%Identification
目的:采用近红外漫反射光谱技术,建立对道地山药的快速无损鉴别方法。方法:收集三个产地(河南、河北、广东)的山药饮片共90份,采集其近红外漫反射光谱。采用判别分析法建立定性鉴别模型,并考察不同数据预处理方法对模型预测结果的影响。结果:道地山药饮片与其他产地的山药饮片在原始光谱与主成分得分的空间分布中均表现出较大的差异性。所建定性判别模型中,经多元散射校正结合二阶导数及SG平滑处理的模型表现出最佳预测结果,其对校正集与验证集的判正率均为100%。结论:近红外漫反射光谱技术在道地药材的质量分析中具有可行性,可实现道地山药饮片的快速无损鉴别。
目的:採用近紅外漫反射光譜技術,建立對道地山藥的快速無損鑒彆方法。方法:收集三箇產地(河南、河北、廣東)的山藥飲片共90份,採集其近紅外漫反射光譜。採用判彆分析法建立定性鑒彆模型,併攷察不同數據預處理方法對模型預測結果的影響。結果:道地山藥飲片與其他產地的山藥飲片在原始光譜與主成分得分的空間分佈中均錶現齣較大的差異性。所建定性判彆模型中,經多元散射校正結閤二階導數及SG平滑處理的模型錶現齣最佳預測結果,其對校正集與驗證集的判正率均為100%。結論:近紅外漫反射光譜技術在道地藥材的質量分析中具有可行性,可實現道地山藥飲片的快速無損鑒彆。
목적:채용근홍외만반사광보기술,건립대도지산약적쾌속무손감별방법。방법:수집삼개산지(하남、하북、엄동)적산약음편공90빈,채집기근홍외만반사광보。채용판별분석법건립정성감별모형,병고찰불동수거예처리방법대모형예측결과적영향。결과:도지산약음편여기타산지적산약음편재원시광보여주성분득분적공간분포중균표현출교대적차이성。소건정성판별모형중,경다원산사교정결합이계도수급SG평활처리적모형표현출최가예측결과,기대교정집여험증집적판정솔균위100%。결론:근홍외만반사광보기술재도지약재적질량분석중구유가행성,가실현도지산약음편적쾌속무손감별。
To investigate the feasibility of NIR spectroscopy in the discrimination of genuine Chinese Yam ,90 samples from three origins were collected and their near infrared diffuse reflectance spectra were acquired.Discriminant analysis was employed to create qualitative model ,and several data pre-processing methods were explored.The results showed that genuine Chinese Yam was greatly different from other samples according to raw spectra and score plot of PCA.The discriminant analysis model with raw spectra after pretreatment of mul-tiplicative scatter correction,2nd derivative and Savitzky -Golay filter smoothing,showed the best predicative ability ( the percentage of correctly identified varieties were both 100%for the calibration sample set and validation sample set ).This research indicated that NIR diffuse reflection spectroscopy could be used for the rapid analysis of genuine Chinese Yam .