合成2,3,4,6-O-四苄基-α-D-葡萄糖三氯乙酰亚胺酯的工艺改进
합성2,3,4,6-O-사변기-α-D-포도당삼록을선아알지적공예개진
Process Improvement on the Synthesis of 2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl Trichloroacetimidate
  • 万方数据
    合成化学 합성화학
    CHINESE JOURNAL OF SYNTHETIC CHEMISTRY
    2013年 3期 333-335,341 ,共4页

    傅大双%张首国%彭涛%温晓雪%颜海燕%王林

    부대쌍%장수국%팽도%온효설%안해연%왕림

    D-葡萄糖%三氯乙酰亚胺酯%合成%工艺改进 D-葡萄糖%三氯乙酰亞胺酯%閤成%工藝改進
    D-포도당%삼록을선아알지%합성%공예개진
    D-glucose%trichloroacetimitate%synthesis%process improvement
    以D-葡萄糖为起始原料,经甲基化、苄基保护和水解,再与三氯乙腈反应合成了2,3,4,6-O-四苄基-α-D-葡萄糖三氯乙酰亚胺酯,总收率44.2％,其结构经1H NMR和ESI-MS确证.
    이D-포도당위기시원료,경갑기화、변기보호화수해,재여삼록을정반응합성료2,3,4,6-O-사변기-α-D-포도당삼록을선아알지,총수솔44.2％,기결구경1H NMR화ESI-MS학증.
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