辐射防护通讯
輻射防護通訊
복사방호통신
RADIATION PROTECTION BULLETIN
2013年
1期
8-11
,共4页
王莉莉%张晔%陆月萍%周彦%曹钟港
王莉莉%張曄%陸月萍%週彥%曹鐘港
왕리리%장엽%륙월평%주언%조종항
210Po%示踪%α能谱%自沉积
210Po%示蹤%α能譜%自沉積
210Po%시종%α능보%자침적
210 Po%Tracer%Alpha spectrometry%Autodeposition
水中痕量210 Po 分析采用的是示踪剂的α能谱分析法。在待分析水样中加入208 Po 示踪剂,以氢氧化铁共沉淀的形式载带钋,在0.5 mol/L 盐酸体系中利用钋对银的高度选择性实现自沉积。利用α谱仪探测系统对样品源测量48 h ,根据钋同位素的对应谱分析210 Po 活度。本文讨论该法与我国现行国标、EML 及 IAEA 分析技术的差异性。
水中痕量210 Po 分析採用的是示蹤劑的α能譜分析法。在待分析水樣中加入208 Po 示蹤劑,以氫氧化鐵共沉澱的形式載帶釙,在0.5 mol/L 鹽痠體繫中利用釙對銀的高度選擇性實現自沉積。利用α譜儀探測繫統對樣品源測量48 h ,根據釙同位素的對應譜分析210 Po 活度。本文討論該法與我國現行國標、EML 及 IAEA 分析技術的差異性。
수중흔량210 Po 분석채용적시시종제적α능보분석법。재대분석수양중가입208 Po 시종제,이경양화철공침정적형식재대박,재0.5 mol/L 염산체계중이용박대은적고도선택성실현자침적。이용α보의탐측계통대양품원측량48 h ,근거박동위소적대응보분석210 Po 활도。본문토론해법여아국현행국표、EML 급 IAEA 분석기술적차이성。
@@@@The determination of 210 Po in water samples was carried out by using of 208 Po tracer with the aid of alpha spectrometry .Adding 208 Po tracer to water samples before preliminary preparation ,the 210 Po and were co-precipitated with iron hydroxide .The polonium were auto-deposited on silver disc by advantage of its high selectiveness in 0 .5 mol/L hydrochloric acid solution .The sample source was counted for 60 hours in al-pha spectrometry system .The determination of 210 Po activity was performed according to different spectra .In addition ,the article discusses the differences of the present analytical method and the national standards ,EML and IAEA methods . 208 Po