火工品
火工品
화공품
INITIATORS & PYROTECHNICS
2014年
1期
38-41
,共4页
叶耀坤%丁锋%严楠%程俊
葉耀坤%丁鋒%嚴楠%程俊
협요곤%정봉%엄남%정준
火药%物理性能%连续测试方法%温度适应性
火藥%物理性能%連續測試方法%溫度適應性
화약%물이성능%련속측시방법%온도괄응성
Pyrotechnic composition%Physical properties%Continuous testing method%Temperature adaptability
针对火药随温度发生的物理变化过程难以连续测试的问题,提出了基于高清数码相机和差示扫描量热仪相结合的方法,将少量松散或压实火药试样置于坩埚中,差示扫描量热仪从常温开始以一定变温速率连续升温或降温,并用高清数码相机拍摄照片连续记录试样物理表观形貌,以实现对火药物理性能随温度变化的连续测试,为火药的安定性分析提供了新途径。
針對火藥隨溫度髮生的物理變化過程難以連續測試的問題,提齣瞭基于高清數碼相機和差示掃描量熱儀相結閤的方法,將少量鬆散或壓實火藥試樣置于坩堝中,差示掃描量熱儀從常溫開始以一定變溫速率連續升溫或降溫,併用高清數碼相機拍攝照片連續記錄試樣物理錶觀形貌,以實現對火藥物理性能隨溫度變化的連續測試,為火藥的安定性分析提供瞭新途徑。
침대화약수온도발생적물리변화과정난이련속측시적문제,제출료기우고청수마상궤화차시소묘량열의상결합적방법,장소량송산혹압실화약시양치우감과중,차시소묘량열의종상온개시이일정변온속솔련속승온혹강온,병용고청수마상궤박섭조편련속기록시양물리표관형모,이실현대화약물이성능수온도변화적련속측시,위화약적안정성분석제공료신도경。
In order to find a solution to continuously test the physical varying process of pyrotechnic composition with temperature change, a method based on the using of digital cameras and differential scanning calorimetry (DSC) was proposed, by putting a small amount of loose or compacted composition in the crucible of DSC, which continuously heat and cool the sample from room temperature at a certain temperature rate, and taking pictures with high-definition digital camera to record the physical appearance of the samples. The method achieves the purpose to test the physical properties of pyrotechnic composition varying with the temperature continuously, as well as provides a new way to analyze the stability of the pyrotechnic composition.