材料研究与应用
材料研究與應用
재료연구여응용
MATERIALS RESEARCH AND APPLICATION
2014年
1期
67-72
,共6页
李翔%刘勇%李光辉%刘牡丹%刘珍珍
李翔%劉勇%李光輝%劉牡丹%劉珍珍
리상%류용%리광휘%류모단%류진진
稀土铌铁粗精矿%还原%添加剂%磁选
稀土鈮鐵粗精礦%還原%添加劑%磁選
희토니철조정광%환원%첨가제%자선
RE-Nb-Fe rough concentrate%reduction roasting%addictive%magnetic separation
采用还原焙烧-磁选工艺,对铁品位31.9%,REO品位3.16%,Nb2 O5品位2.91%的稀土铌铁粗精矿进行分离回收铁和稀土、铌的研究.结果表明:在硫酸钠活性炭粉添加质量分数分别为15%和5%、还原焙烧温度为1100℃、还原焙烧时间为120 min的条件下,对稀土铌铁预富集粗精矿进行还原焙烧.然后在还原焙烧产物磨矿细度为-0.074 mm占85.4%,磁选强度为80 mT的条件下进行磁选,最终可获得铁品位89.32%、回收率91.47%的金属铁粉,稀土、铌富集物的REO ,Nb2 O5品位分别为5.36%和4.62%,回收率分别为96.09%和95.83%的指标.实现了稀土铌铁粗精矿中铁和稀土、铌的有效分离和回收.
採用還原焙燒-磁選工藝,對鐵品位31.9%,REO品位3.16%,Nb2 O5品位2.91%的稀土鈮鐵粗精礦進行分離迴收鐵和稀土、鈮的研究.結果錶明:在硫痠鈉活性炭粉添加質量分數分彆為15%和5%、還原焙燒溫度為1100℃、還原焙燒時間為120 min的條件下,對稀土鈮鐵預富集粗精礦進行還原焙燒.然後在還原焙燒產物磨礦細度為-0.074 mm佔85.4%,磁選彊度為80 mT的條件下進行磁選,最終可穫得鐵品位89.32%、迴收率91.47%的金屬鐵粉,稀土、鈮富集物的REO ,Nb2 O5品位分彆為5.36%和4.62%,迴收率分彆為96.09%和95.83%的指標.實現瞭稀土鈮鐵粗精礦中鐵和稀土、鈮的有效分離和迴收.
채용환원배소-자선공예,대철품위31.9%,REO품위3.16%,Nb2 O5품위2.91%적희토니철조정광진행분리회수철화희토、니적연구.결과표명:재류산납활성탄분첨가질량분수분별위15%화5%、환원배소온도위1100℃、환원배소시간위120 min적조건하,대희토니철예부집조정광진행환원배소.연후재환원배소산물마광세도위-0.074 mm점85.4%,자선강도위80 mT적조건하진행자선,최종가획득철품위89.32%、회수솔91.47%적금속철분,희토、니부집물적REO ,Nb2 O5품위분별위5.36%화4.62%,회수솔분별위96.09%화95.83%적지표.실현료희토니철조정광중철화희토、니적유효분리화회수.
Fe ,RE ,Nb separation and recovery from RE-Nb-Fe rough concentrate with total iron grade of 31 .9% ,REO grade of 3 .16% and Nb2 O5 grade of 2 .91% was studied by reduction roasting-magnetic sepa-ration .It was found that metallic iron powder with total iron grade of 89 .32% and the iron recovery of 91 .47% were obtained when RE-NB-Fe enrichment rough concentrate was reduction roasted first at 1100℃ for 120 min using sodium sulfate dosage about 15% ,then magnetic separated using the grinding fineness of ores less than 0 .074 mm 85 .4% and the magnetic field intensity about 800 mT .REO grade is 5 .36% and Nb2 O5 grade is 4 .62% in rare earth ,niobium concentrate with the REO recovery of 96 .09%and the Nb2O5 recovery of 95 .83% .The effective separation and recovery of iron ,rare-earth and niobium from RE-Nb-Fe associated rough concentrate was carried out .