信阳师范学院学报（自然科学版）
信暘師範學院學報（自然科學版）
신양사범학원학보（자연과학판）
JOURNAL OF XINYANG NORMAL UNIVERSITY(NATURAL SCIENCE EDITION)
2013年
3期
407-410
,共4页
栗印环%张秀兰%宋信虹%闫小舍
慄印環%張秀蘭%宋信虹%閆小捨
률인배%장수란%송신홍%염소사
超声波辅助%粉煤灰%淀粉%复合材料%吸水保水
超聲波輔助%粉煤灰%澱粉%複閤材料%吸水保水
초성파보조%분매회%정분%복합재료%흡수보수
ultrasonic assisted%fly ash%starch%composite%water absorption and retention
利用超声波辅助合成粉煤灰／淀粉吸水保水复合材料，考察了粉煤灰、淀粉、交联剂、引发剂及中和度等因素对复合材料吸水倍率的影响，用 X－射线衍射及红外光谱分析样品的微观结构．结果表明：粉煤灰、淀粉与丙烯酸交联聚合良好．当粉煤灰、淀粉、交联剂和引发剂用量分别为丙烯酸单体质量的10％、5％、0．11％和0．20％，中和度为80％，反应温度为80℃时，复合材料吸自来水倍率达571．6 g／g ，吸 NaCl 水溶液倍率达74．5 g／g．
利用超聲波輔助閤成粉煤灰／澱粉吸水保水複閤材料，攷察瞭粉煤灰、澱粉、交聯劑、引髮劑及中和度等因素對複閤材料吸水倍率的影響，用 X－射線衍射及紅外光譜分析樣品的微觀結構．結果錶明：粉煤灰、澱粉與丙烯痠交聯聚閤良好．噹粉煤灰、澱粉、交聯劑和引髮劑用量分彆為丙烯痠單體質量的10％、5％、0．11％和0．20％，中和度為80％，反應溫度為80℃時，複閤材料吸自來水倍率達571．6 g／g ，吸 NaCl 水溶液倍率達74．5 g／g．
이용초성파보조합성분매회／정분흡수보수복합재료，고찰료분매회、정분、교련제、인발제급중화도등인소대복합재료흡수배솔적영향，용 X－사선연사급홍외광보분석양품적미관결구．결과표명：분매회、정분여병희산교련취합량호．당분매회、정분、교련제화인발제용량분별위병희산단체질량적10％、5％、0．11％화0．20％，중화도위80％，반응온도위80℃시，복합재료흡자래수배솔체571．6 g／g ，흡 NaCl 수용액배솔체74．5 g／g．
The water absorbing-retention composite of flyash /starch was prepared by ultrasonic assisted .The influ-ence factors to the absorbancy, which included fly ash, starch, crosslinker, initiator and degree of neutralization , were investigated.The structure of the samples was characterized by X -ray diffraction and infrared spectroscope.The results showed that there are strong chemical interactions of ionic crosslinking polymerization between fly ash , starch and a-crylic.When the amount of fly ash, starch, crosslinker and initiator, accounting for 10%, 5%, 0.11%, 0.20% of the monomer mass, the neutralization degree is 80%,the reaction temperature is 80 ℃,the absorbancy of the composite to tap water and 0.9%NaCl solution is 571.6 g/g and 74.5 g/g respectively.
