CAJ | 학술논문

目的：制定化瘀通络健盘贴的质量标准。方法采用薄层色谱（TLC）法对处方中乳香、没药和血竭进行定性鉴别；采用高效液相色谱（HPLC）法对血竭中的血竭素进行含量测定。结果薄层色谱专属性强、斑点清晰、分离度好；血竭素进样量在0.130～0.455μg范围内具有良好线性关系，回归方程为：Y=5557853187X-49712，r=0.9997；加样回收率平均值为98.49%，RSD为1.61%（n=6）。结论该方法简便、检测灵敏度高、重现性好，可用于化瘀通络健盘贴的质量控制。
목적：제정화어통락건반첩적질량표준。방법채용박층색보（TLC）법대처방중유향、몰약화혈갈진행정성감별；채용고효액상색보（HPLC）법대혈갈중적혈갈소진행함량측정。결과박층색보전속성강、반점청석、분리도호；혈갈소진양량재0.130～0.455μg범위내구유량호선성관계，회귀방정위：Y=5557853187X-49712，r=0.9997；가양회수솔평균치위98.49%，RSD위1.61%（n=6）。결론해방법간편、검측령민도고、중현성호，가용우화어통락건반첩적질량공제。
Objective To formulate Huayu Tongluo Jianpan Stickers to the quality control stan-dards. Methods To use thin layer chromatography to identify the Frankincense、Myrrh and Dragon's blood. Use high performance liquid chromatography method for the determination of dr-acorhodin content. Results The TLC is a feasible method with strong specificity, TLC spots were clear and good separation;Dracorhodinin 0.130~0.455μg has a good linear relationship. The regression equation is Y=6E+09X-49712, r=0.9997. Average sample recovery rate was 98.49%, RSD was 1.61%(n=6).Conclusion The method is simple, high detection sensitivity,good reproducibility,and can be used for quality control of Huayu Tongluo Jianpan Stickers.