应用化工
應用化工
응용화공
APPLIED CHEMICAL INDUSTRY
2014年
6期
1047-1049
,共3页
卫向南%李伟光%刘雄民%陈帅棠%谢霜%黄燕香%董烈%黄强
衛嚮南%李偉光%劉雄民%陳帥棠%謝霜%黃燕香%董烈%黃彊
위향남%리위광%류웅민%진수당%사상%황연향%동렬%황강
肉桂叶%水扩散蒸馏%肉桂油%GC-MS 分析
肉桂葉%水擴散蒸餾%肉桂油%GC-MS 分析
육계협%수확산증류%육계유%GC-MS 분석
cinnamon leaf%hydro-diffusion distillation%cinnamon oil%GC-MS analyze
以肉桂叶为原料,在5 L 不锈钢蒸馏釜中采用水扩散蒸馏提取肉桂油,考察了蒸馏时间、投料量、进口压力3个因素对肉桂油得油率的影响。结果表明,水扩散提取的适宜条件为:蒸馏时间90 min,投料量200 g/ L,蒸汽进口压力为1750 Pa,此时得油率为8.88‰,肉桂油的主要成分为肉桂醛(86.89%)、苯甲醛(1.55%)、乙酸肉桂酯(3.92%)、邻甲氧基肉桂醛(4.56%)。
以肉桂葉為原料,在5 L 不鏽鋼蒸餾釜中採用水擴散蒸餾提取肉桂油,攷察瞭蒸餾時間、投料量、進口壓力3箇因素對肉桂油得油率的影響。結果錶明,水擴散提取的適宜條件為:蒸餾時間90 min,投料量200 g/ L,蒸汽進口壓力為1750 Pa,此時得油率為8.88‰,肉桂油的主要成分為肉桂醛(86.89%)、苯甲醛(1.55%)、乙痠肉桂酯(3.92%)、鄰甲氧基肉桂醛(4.56%)。
이육계협위원료,재5 L 불수강증류부중채용수확산증류제취육계유,고찰료증류시간、투료량、진구압력3개인소대육계유득유솔적영향。결과표명,수확산제취적괄의조건위:증류시간90 min,투료량200 g/ L,증기진구압력위1750 Pa,차시득유솔위8.88‰,육계유적주요성분위육계철(86.89%)、분갑철(1.55%)、을산육계지(3.92%)、린갑양기육계철(4.56%)。
Cinnamon leaf as the major raw materials and cinnamon oil was extracted by hydro-diffusion distillation method in a 5 L stainless still. Effect of distillation time,material inventory and inlet steam pressure on cinnamon oil rate were investigated. The results showed that the extraction time was optimized to 90 min and the optimal inventory of the material is 200 g / L and the best inlet steam pressure is 1 750 Pa,under these conditions,the extraction rate can reach 8. 88‰. The oil extracted by hydro-diffu-sion distillation is made of four major components-cinnamal dehyde( 86. 89% ),benzoic aldehyde (1. 55% ),cinnamyl acetate(3. 92% ),methoxy cinnamyl dehyde(4. 56% ).