CAJ | 학술논문

目的：建立新疆昆仑雪菊中柠檬烯含量的测定方法。方法采用气相色谱法，Rtx-5石英毛细管柱(30 m×0.25 mm，0.25μm)；程序升温院50℃保持5 min，以10℃/min升至230℃，保持10 min；载气流量院18.30 mL/min；柱压院100 kPa；进样口温度院250℃；分流比院10：1；进样量院1μL。结果柠檬烯在41.90~251.40μg/mL范围内线性关系良好(r =0.9996，n =6)，平均回收率为102.72豫，RSD为1.35%(n =9)。结论本实验方法可靠，重复性好，专属性强，可用于雪菊挥发油中柠檬烯的含量测定，以控制雪菊挥发油的质量。
목적：건립신강곤륜설국중저몽희함량적측정방법。방법채용기상색보법，Rtx-5석영모세관주(30 m×0.25 mm，0.25μm)；정서승온원50℃보지5 min，이10℃/min승지230℃，보지10 min；재기류량원18.30 mL/min；주압원100 kPa；진양구온도원250℃；분류비원10：1；진양량원1μL。결과저몽희재41.90~251.40μg/mL범위내선성관계량호(r =0.9996，n =6)，평균회수솔위102.72예，RSD위1.35%(n =9)。결론본실험방법가고，중복성호，전속성강，가용우설국휘발유중저몽희적함량측정，이공제설국휘발유적질량。
Objective To establish a method for determination of limonene in Xinjiang Kunlun Chrysanthemum by GC. Methods The GC equipped with FID detector, and a Rtx-5 capillary column were used (30 mí0.25 mm, 0.25μm). The temperature program of column oven was set as follows:50℃for 5 min, increased to 230℃at a rate of 10℃/min, held for 10 min. The carrier gas flow rate:18.30 mL/min;column press:100 kPa;injection port temperature:250℃;split ration:10:1;sample volume:1μL. Results Limonene was linear in the range of 41.90-251.40μg/mL (r=0.9996, n=6). The average recovery was 102.72%(n=9), and RSD was 1.35%. Conclusion The method can be used to determine the con-tent of limonene in Xinjiang Kunlun Chrysanthemum, in order to control the quality of volatile oil from Chrysanthemum.