马钱苷的NMR数据解析
마전감적NMR수거해석
An NMR Study on Chrysathain
  • 万方数据
    河南科学 하남과학
    HENAN SCIENCE
    2014年 9期 1703-1705 ,共3页

    范毅%张海艳%李坤威%张剑%赵天增

    범의%장해염%리곤위%장검%조천증

    NMR%归属%NOESY%马钱苷 NMR%歸屬%NOESY%馬錢苷
    NMR%귀속%NOESY%마전감
    NMR%assignment%NOESY%loganin
    通过DEPT及1H-1HCOSY，HSQC，HMBC，NOESY等2D NMR技术，对环烯醚萜苷化合物--马钱苷的1H和13C NMR信号进行了详细解析和全归属，尤其利用NOESY技术确证了其立体结构。
    통과DEPT급1H-1HCOSY，HSQC，HMBC，NOESY등2D NMR기술，대배희미첩감화합물--마전감적1H화13C NMR신호진행료상세해석화전귀속，우기이용NOESY기술학증료기입체결구。
    Loganin,an important iro doid,was usually isolated from Cornus officinalis Sieb,et Zucc. and Lonicera chrysatha Thunb.. The 1H and 13C NMR chemical shifts of loganin were completely assigned by using a combination of 1D NMR(1H,13C NMR and DEPT)and 2D NMR(1H- 1H COSY,HSQC,HMBC and NOESY)techniques, especially its stereoscopic strcture was studied with NOESY.
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