功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
18期
18092-18095,18098
,共5页
罗林%介万奇%徐亚东%傅莉
囉林%介萬奇%徐亞東%傅莉
라림%개만기%서아동%부리
缺陷闪锌矿%空位%孪晶%EBSD%HRTEM
缺陷閃鋅礦%空位%孿晶%EBSD%HRTEM
결함섬자광%공위%련정%EBSD%HRTEM
defect zinc-blende%vacancy%twin%EBSD%HRTEM
通过电子背散射衍射(EBSD)和高分辨透射电子显微术(HRTEM)对缺陷闪锌矿晶体 Hg3 In2 Te6(MIT)中的孪晶进行观察。实验发现,大多数基体的应变能比孪晶小,且一些带状孪晶的所有孪晶界均不共格。此外,高密度结构空位的存在并未改变孪生面和孪生方向。上述结果可按照变形孪晶,并考虑高密度结构空位团簇的影响来解释。HRTEM观察显示孪晶界上存在着台阶和孪生位错,符合变形孪晶的特征。
通過電子揹散射衍射(EBSD)和高分辨透射電子顯微術(HRTEM)對缺陷閃鋅礦晶體 Hg3 In2 Te6(MIT)中的孿晶進行觀察。實驗髮現,大多數基體的應變能比孿晶小,且一些帶狀孿晶的所有孿晶界均不共格。此外,高密度結構空位的存在併未改變孿生麵和孿生方嚮。上述結果可按照變形孿晶,併攷慮高密度結構空位糰簇的影響來解釋。HRTEM觀察顯示孿晶界上存在著檯階和孿生位錯,符閤變形孿晶的特徵。
통과전자배산사연사(EBSD)화고분변투사전자현미술(HRTEM)대결함섬자광정체 Hg3 In2 Te6(MIT)중적련정진행관찰。실험발현,대다수기체적응변능비련정소,차일사대상련정적소유련정계균불공격。차외,고밀도결구공위적존재병미개변련생면화련생방향。상술결과가안조변형련정,병고필고밀도결구공위단족적영향래해석。HRTEM관찰현시련정계상존재착태계화련생위착,부합변형련정적특정。
Electron backscattered diffraction (EBSD ) and high-resolution transmission electron microscopy (HRTEM)are used to study the twins in Hg3 In2 Te6 (MIT)crystals with defect zinc-blende structure.The re-sults show that strain energy of the maj ority of matrices was smaller than that of their corresponding twins.All twin boundaries of some band-like twins are incoherent.In addition,the existence of high-density structural va-cancies do not change the twinning plane and the twinning direction.The above results can be explained by de-formation twins with the consideration on the influence of high-density structural vacancy clusters.HRTEM observation shows that steps and twinning dislocations exist at the twin boundaries,which are consistent with deformation twins.