中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
2期
210-214
,共5页
苏华%史方超%乔立业%陆崟%任海祥
囌華%史方超%喬立業%陸崟%任海祥
소화%사방초%교립업%륙음%임해상
黄芩%黄芩苷%紫外辐射%正交试验
黃芩%黃芩苷%紫外輻射%正交試驗
황금%황금감%자외복사%정교시험
Radix scutellariae%Baicalin%Ultraviolet radiation(UVR)%Orthogonal design
目的::研究黄芩防晒成分最佳提取工艺。方法:采用紫外分光光度法检测黄芩提取液在200~400 nm各区的紫外吸收率,采用高效液相色谱法测定黄芩苷含量。分别以黄芩提取液紫外吸收率,黄芩浸膏得率,黄芩苷提取量为指标,采用单因素考察和正交试验,确定黄芩防晒成分提取工艺。结果:黄芩提取液的最佳提取工艺为:提取乙醇浓度60%,料液比1∶40,超声时间40 min,超声温度60℃。结论:黄芩提取液在紫外线中波范围有很强的吸收,具很好的防晒作用。超声波提取法简单,合理,可行,可用于黄芩防晒成分的提取。
目的::研究黃芩防曬成分最佳提取工藝。方法:採用紫外分光光度法檢測黃芩提取液在200~400 nm各區的紫外吸收率,採用高效液相色譜法測定黃芩苷含量。分彆以黃芩提取液紫外吸收率,黃芩浸膏得率,黃芩苷提取量為指標,採用單因素攷察和正交試驗,確定黃芩防曬成分提取工藝。結果:黃芩提取液的最佳提取工藝為:提取乙醇濃度60%,料液比1∶40,超聲時間40 min,超聲溫度60℃。結論:黃芩提取液在紫外線中波範圍有很彊的吸收,具很好的防曬作用。超聲波提取法簡單,閤理,可行,可用于黃芩防曬成分的提取。
목적::연구황금방쇄성분최가제취공예。방법:채용자외분광광도법검측황금제취액재200~400 nm각구적자외흡수솔,채용고효액상색보법측정황금감함량。분별이황금제취액자외흡수솔,황금침고득솔,황금감제취량위지표,채용단인소고찰화정교시험,학정황금방쇄성분제취공예。결과:황금제취액적최가제취공예위:제취을순농도60%,료액비1∶40,초성시간40 min,초성온도60℃。결론:황금제취액재자외선중파범위유흔강적흡수,구흔호적방쇄작용。초성파제취법간단,합리,가행,가용우황금방쇄성분적제취。
Objective:To optimize the extraction technology of radix scutellariae. Methods: The extraction of radix scutellariae was scanned by ultraviolet spectrophotometry from 200 to 400nm. The content of baicalin was determined by HPLC. The ultraviolet ab-sorption, baicalin content and extraction rate were used as the indices, and the optimal extraction conditions were investigated by single factor experiments and orthogonal design tests. Results: The optimal extraction conditions were as follows: the ethanol concentration was 60%, the solid-liquid ratio was 1∶40, ultrasound extraction time and temperature was 40 min and 60℃, respectively. Conclusion:The extraction of radix scutellariae has good sunscreen with promising ultraviolet absorption in UVB. Ultrasound extraction has high ex-traction yield with short time, which can be used to extract sun-screening constituents from radix scutellariae.