中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
2期
343-345
,共3页
血竭素%高效液相色谱法%含量测定%骨伤跌打止痛胶囊
血竭素%高效液相色譜法%含量測定%骨傷跌打止痛膠囊
혈갈소%고효액상색보법%함량측정%골상질타지통효낭
Dracorhodin%HPLC%Determination%Gushang Dieda Zhitong capsules
目的：：建立骨伤跌打止痛胶囊中血竭素的含量测定方法。方法：采用HPLC法,色谱柱为Shimadzu VP-ODS C18(250 mm ×4.6 mm,5μm),流动相为乙腈-0.05 mol·L-1磷酸二氢钠溶液(35∶65),检测波长为440 nm,流速为1.0 ml·min-1。柱温为30℃。结果：血竭素线性范围为0.047~0.234μg,r=0.9999,平均加样回收率为99.9%,RSD为1.5%。结论：本法操作简便、快速、准确可靠,专属性强,可作为骨伤跌打止痛胶囊的质量控制方法。
目的：：建立骨傷跌打止痛膠囊中血竭素的含量測定方法。方法：採用HPLC法,色譜柱為Shimadzu VP-ODS C18(250 mm ×4.6 mm,5μm),流動相為乙腈-0.05 mol·L-1燐痠二氫鈉溶液(35∶65),檢測波長為440 nm,流速為1.0 ml·min-1。柱溫為30℃。結果：血竭素線性範圍為0.047~0.234μg,r=0.9999,平均加樣迴收率為99.9%,RSD為1.5%。結論：本法操作簡便、快速、準確可靠,專屬性彊,可作為骨傷跌打止痛膠囊的質量控製方法。
목적：：건립골상질타지통효낭중혈갈소적함량측정방법。방법：채용HPLC법,색보주위Shimadzu VP-ODS C18(250 mm ×4.6 mm,5μm),류동상위을정-0.05 mol·L-1린산이경납용액(35∶65),검측파장위440 nm,류속위1.0 ml·min-1。주온위30℃。결과：혈갈소선성범위위0.047~0.234μg,r=0.9999,평균가양회수솔위99.9%,RSD위1.5%。결론：본법조작간편、쾌속、준학가고,전속성강,가작위골상질타지통효낭적질량공제방법。
Objective:To establish a method to determine dracorhodin in Gushang Dieda Zhitong capsules by HPLC. Methods:An HPLC method was used for the determination of dracorhodin, a Shimadzu VP-ODS C18 column was used,and acetonitrile-0. 05 mol ·L-1 sodium dihydrogen phosphate solution(35∶65)was the mobile phase. The flow rate was 1.0 ml·min-1. The detection wave-length was at 440nm. Results:The linear range of dracorhodin was 0. 047-0. 234 μg(r=0. 999 9). The average recovery was 99. 9%with RSD of 1. 5%. Conclusion:The method is simple, rapid, accurate and specific. It can be used in the quality control of Gushang Dieda Zhitong capsules.
