食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2014年
10期
66-69
,共4页
刘鑫%谭烨%周红审%王昊
劉鑫%譚燁%週紅審%王昊
류흠%담엽%주홍심%왕호
甜橙%水蒸气蒸馏%气相色谱-质谱法%卷烟加香
甜橙%水蒸氣蒸餾%氣相色譜-質譜法%捲煙加香
첨등%수증기증류%기상색보-질보법%권연가향
sweet orange%steam distillation%GC-MS%cigarette flavoring
采用水蒸气蒸馏法制备甜橙油,研究了物料比、提取温度、提取时间等因素对甜橙油得率的影响,进行最佳工艺优化,并以气相色谱-质谱法(GC-MS)对其化学成分进行分离和鉴定。结果表明,其最佳工艺条件为:物料比1/8、提取温度130℃、提取时间8 h,精油得率为0.495%;甜橙油主要成分为柠檬油精(93.00%)、芳樟醇(1.52%)、月桂烯(1.49%)、辛醛(0.42%)、α-蒎烯(0.39%)等物质;将该香料用于卷烟加香,能够明显丰富烟香,减轻刺激,甜润烟气,改善卷烟余味。
採用水蒸氣蒸餾法製備甜橙油,研究瞭物料比、提取溫度、提取時間等因素對甜橙油得率的影響,進行最佳工藝優化,併以氣相色譜-質譜法(GC-MS)對其化學成分進行分離和鑒定。結果錶明,其最佳工藝條件為:物料比1/8、提取溫度130℃、提取時間8 h,精油得率為0.495%;甜橙油主要成分為檸檬油精(93.00%)、芳樟醇(1.52%)、月桂烯(1.49%)、辛醛(0.42%)、α-蒎烯(0.39%)等物質;將該香料用于捲煙加香,能夠明顯豐富煙香,減輕刺激,甜潤煙氣,改善捲煙餘味。
채용수증기증류법제비첨등유,연구료물료비、제취온도、제취시간등인소대첨등유득솔적영향,진행최가공예우화,병이기상색보-질보법(GC-MS)대기화학성분진행분리화감정。결과표명,기최가공예조건위:물료비1/8、제취온도130℃、제취시간8 h,정유득솔위0.495%;첨등유주요성분위저몽유정(93.00%)、방장순(1.52%)、월계희(1.49%)、신철(0.42%)、α-파희(0.39%)등물질;장해향료용우권연가향,능구명현봉부연향,감경자격,첨윤연기,개선권연여미。
The research aimed to study the extraction of sweet orange oil by steam distillation. The effects of adding water, distilling temperature, distilling time on the extraction rate were studied, and by GC-MS on its chemical constituents were separated and identified. The results show that the optimum extraction technological conditions of sweet orange oil as follows:Adding water 8 times, distilling temperature 130℃, and distilling time 8 h. The extraction rate was 0.495%. The main components were efficiently separated and detected , including limonene, linalool, Myrcene, Octanal, pinene, etc. these products could be enrich the tobacco flavor, reduce the irritancy of smoke and improve sweet taste obviously by directly adding to the tobacco.