中国有色金属学报
中國有色金屬學報
중국유색금속학보
THE CHINESE JOURNAL OF NONFERROUS METALS
2014年
9期
2228-2234
,共7页
曾世宝%叶凌英%刘胜胆%邬沛卿%单朝军%邓运来%张新明
曾世寶%葉凌英%劉勝膽%鄔沛卿%單朝軍%鄧運來%張新明
증세보%협릉영%류성담%오패경%단조군%산운래%장신명
7N01铝合金%Al 3 Zr%均匀化%升温速率%再结晶%力学性能
7N01鋁閤金%Al 3 Zr%均勻化%升溫速率%再結晶%力學性能
7N01려합금%Al 3 Zr%균균화%승온속솔%재결정%역학성능
7N01 aluminum alloy%Al3Zr%homogenization%heating rate%recrystallization%mechanical property
采用光学显微镜、扫描电镜、电子探针显微镜、透射电镜和常温拉伸等测试方法研究均匀化升温速率对7N01铝合金显微组织和力学性能的影响。结果表明:与升温速率较快的均匀化制度相比,采用升温速率小于100℃/h 的慢速升温均匀化制度更有利于细小弥散Al 3 Zr粒子的析出,使Al 3 Zr粒子分布均匀;细小弥散的Al 3 Zr粒子能有效地阻止再结晶晶界的迁移,抑制再结晶的发生。随着均匀化升温速率由500℃/h降低到20℃/h,析出的Al 3 Zr粒子数量增加,尺寸减小,析出相体积分数和半径的比值φ/r由75.8μm-1增大到359.1μm-1,使得Al 3 Zr粒子对晶界的钉扎力增大,因此合金的再结晶分数相应地由31.92%逐渐降低到1.32%;保留下来的大量位错和未再结晶组织提高了合金的综合力学性能。
採用光學顯微鏡、掃描電鏡、電子探針顯微鏡、透射電鏡和常溫拉伸等測試方法研究均勻化升溫速率對7N01鋁閤金顯微組織和力學性能的影響。結果錶明:與升溫速率較快的均勻化製度相比,採用升溫速率小于100℃/h 的慢速升溫均勻化製度更有利于細小瀰散Al 3 Zr粒子的析齣,使Al 3 Zr粒子分佈均勻;細小瀰散的Al 3 Zr粒子能有效地阻止再結晶晶界的遷移,抑製再結晶的髮生。隨著均勻化升溫速率由500℃/h降低到20℃/h,析齣的Al 3 Zr粒子數量增加,呎吋減小,析齣相體積分數和半徑的比值φ/r由75.8μm-1增大到359.1μm-1,使得Al 3 Zr粒子對晶界的釘扎力增大,因此閤金的再結晶分數相應地由31.92%逐漸降低到1.32%;保留下來的大量位錯和未再結晶組織提高瞭閤金的綜閤力學性能。
채용광학현미경、소묘전경、전자탐침현미경、투사전경화상온랍신등측시방법연구균균화승온속솔대7N01려합금현미조직화역학성능적영향。결과표명:여승온속솔교쾌적균균화제도상비,채용승온속솔소우100℃/h 적만속승온균균화제도경유리우세소미산Al 3 Zr입자적석출,사Al 3 Zr입자분포균균;세소미산적Al 3 Zr입자능유효지조지재결정정계적천이,억제재결정적발생。수착균균화승온속솔유500℃/h강저도20℃/h,석출적Al 3 Zr입자수량증가,척촌감소,석출상체적분수화반경적비치φ/r유75.8μm-1증대도359.1μm-1,사득Al 3 Zr입자대정계적정찰력증대,인차합금적재결정분수상응지유31.92%축점강저도1.32%;보류하래적대량위착화미재결정조직제고료합금적종합역학성능。
The effects of homogenization heating rate on the microstructure and mechanical properties of 7N01 aluminum alloy were investigated by optical microscopy (OM), scanning electron microcopy (SEM), electron probe microanalyzer (EPMA), transmission electron microcopy (TEM) and tensile test. The results show that using a slow homogenization heating rate less than 100 ℃/h is favorable for the precipitation of fine and uniformly distributed Al3Zr particles compared with fast homogenization heating rate. The dispersion distribution of fine Al3Zr particles can decrease the recrystallized fraction since the Al3Zr particles can effectively prevent the migration of recrystallization grain boundary. When the homogenization heating rate decreases from 500℃/h to 20℃/h, the average dispersoid number increases, the particle size decreases, and the ratio of volume fraction (φ) to radius (r) of the precipitate (φ/r) increases from 75.8μm-1 to 359.1 μm-1, which improves the dragging effect of Al3Zr particles on the grain boundaries and leads to a reduction in the recrystallized fraction from 31.92% to 1.32%. Meanwhile, the unrecrystallized microstructures containing profuse dislocations enhance the comprehensive mechanical properties of the studied alloy.