中国药业
中國藥業
중국약업
CHINA PHARMACEUTICALS
2014年
16期
56-57
,共2页
黄海%施家辉%李咏华%黄建军
黃海%施傢輝%李詠華%黃建軍
황해%시가휘%리영화%황건군
甲基橙皮苷%喷雾干燥%溶剂残留量%正交试验
甲基橙皮苷%噴霧榦燥%溶劑殘留量%正交試驗
갑기등피감%분무간조%용제잔류량%정교시험
methyl hesperidin%spray drying technology%solvent residual amount%orthogonal experiment
目的：优选甲基橙皮苷喷雾干燥的最佳工艺。方法采用正交试验法，以溶剂残留量和收率为考察指标，考察进风温度、出风温度和塔内压力的影响。结果甲基橙皮苷喷雾干燥的最佳工艺为进风温度170℃，出风温度85℃，塔内压力-7 Pa。干燥所得的甲基橙皮苷的平均溶剂残留量为3050 mg / kg，平均收率为93.6%。结论该试验优选的工艺稳定，能有效控制产品的质量。
目的：優選甲基橙皮苷噴霧榦燥的最佳工藝。方法採用正交試驗法，以溶劑殘留量和收率為攷察指標，攷察進風溫度、齣風溫度和塔內壓力的影響。結果甲基橙皮苷噴霧榦燥的最佳工藝為進風溫度170℃，齣風溫度85℃，塔內壓力-7 Pa。榦燥所得的甲基橙皮苷的平均溶劑殘留量為3050 mg / kg，平均收率為93.6%。結論該試驗優選的工藝穩定，能有效控製產品的質量。
목적：우선갑기등피감분무간조적최가공예。방법채용정교시험법，이용제잔류량화수솔위고찰지표，고찰진풍온도、출풍온도화탑내압력적영향。결과갑기등피감분무간조적최가공예위진풍온도170℃，출풍온도85℃，탑내압력-7 Pa。간조소득적갑기등피감적평균용제잔류량위3050 mg / kg，평균수솔위93.6%。결론해시험우선적공예은정，능유효공제산품적질량。
Objective To optimize the spray drying technology of methyl hesperidin. Methods By using the orthogonal experiment method and with the solvent residual amount and yield as the investigation indexes,the influences of inlet air temperature,outlet air temperature and tower pressure were investigated. Results The optimum technology of methyl hesperidin spray drying was the inlet air temperature of 170 ℃ ,outlet air temperature of 85 ℃ ,tower pressure of - 7 Pa,the average solvent residual amount in methyl hes-peridin obtained by drying was 3 050 ppm and the average yield was 93. 6% . Conclusion The technology screened by this experiment is stable and can effectively control the quality of the products.
