香料香精化妆品
香料香精化妝品
향료향정화장품
FLAVOUR FRAGRANCE COSMETICS
2014年
3期
31-32,58
,共3页
董爱君%刘华臣%庞登红%张磊%吴昭
董愛君%劉華臣%龐登紅%張磊%吳昭
동애군%류화신%방등홍%장뢰%오소
干布枯叶%挥发成分分析%气相色谱-质谱联用分析%水蒸气蒸馏法
榦佈枯葉%揮髮成分分析%氣相色譜-質譜聯用分析%水蒸氣蒸餾法
간포고협%휘발성분분석%기상색보-질보련용분석%수증기증류법
dry Buchu leaf%analysis of volatile component%GC-MS%steam distillation
采用水蒸气蒸馏法,对干布枯叶中挥发油进行提取,测得干布枯叶中的挥发油提取率为0.3‰。并用气相色谱-质谱联用技术对挥发成分进行分析鉴定,鉴定出23种化学成分,应用峰面积归一化法确定了各成分的相对百分比。水蒸气蒸馏法提取的干布枯叶挥发油中主要含棕榈酸(38.49%)、亚油酸(36.80%)、叶绿醇(4.64%)、硬脂酸(4.27%)、植酮(2.35%)、肉豆蔻酸(1.38%)等。
採用水蒸氣蒸餾法,對榦佈枯葉中揮髮油進行提取,測得榦佈枯葉中的揮髮油提取率為0.3‰。併用氣相色譜-質譜聯用技術對揮髮成分進行分析鑒定,鑒定齣23種化學成分,應用峰麵積歸一化法確定瞭各成分的相對百分比。水蒸氣蒸餾法提取的榦佈枯葉揮髮油中主要含棕櫚痠(38.49%)、亞油痠(36.80%)、葉綠醇(4.64%)、硬脂痠(4.27%)、植酮(2.35%)、肉豆蔻痠(1.38%)等。
채용수증기증류법,대간포고협중휘발유진행제취,측득간포고협중적휘발유제취솔위0.3‰。병용기상색보-질보련용기술대휘발성분진행분석감정,감정출23충화학성분,응용봉면적귀일화법학정료각성분적상대백분비。수증기증류법제취적간포고협휘발유중주요함종려산(38.49%)、아유산(36.80%)、협록순(4.64%)、경지산(4.27%)、식동(2.35%)、육두구산(1.38%)등。
The volatile oil was obtained from dry Buchu leaf by steam distillation method with the yield of 0 .3‰ . Twenty-three components were identified by GC-MS,the relative contents of which were determined with area normalization method. The results showed that the main components in oil of dry buchu leaf were hexadecanoic acid (38. 49% ),linoleic acid (36.80% ),phytol (4.64% ),octadecanoic acid (4.27% ),perhydrofarnesyl acetone (2.35% ),and myristic acid (1 .38% ).