食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2014年
14期
79-82
,共4页
虾干%近红外光谱%磺胺嘧啶%二甲基磺胺嘧啶%无损检测
蝦榦%近紅外光譜%磺胺嘧啶%二甲基磺胺嘧啶%無損檢測
하간%근홍외광보%광알밀정%이갑기광알밀정%무손검측
Prawn%NIRS%sulfadiazine%sulfamethazine%non-destructive determination
通过虾干的近红外反射光谱与拟合其中所含磺胺药物含量，建立近红外定量模型，用于虾干中磺胺药物快速无损检测。模型采用偏最小二乘法（PLS）拟合，磺胺嘧啶和磺胺二甲基嘧啶的定标模型相关系数分别达0.98和0.94以上。模型的标准偏差（RMSECV）<6%，表明该模型能准确快速地测定虾干中的磺胺嘧啶和磺胺二甲基嘧啶含量，且可用于实际生产中。
通過蝦榦的近紅外反射光譜與擬閤其中所含磺胺藥物含量，建立近紅外定量模型，用于蝦榦中磺胺藥物快速無損檢測。模型採用偏最小二乘法（PLS）擬閤，磺胺嘧啶和磺胺二甲基嘧啶的定標模型相關繫數分彆達0.98和0.94以上。模型的標準偏差（RMSECV）<6%，錶明該模型能準確快速地測定蝦榦中的磺胺嘧啶和磺胺二甲基嘧啶含量，且可用于實際生產中。
통과하간적근홍외반사광보여의합기중소함광알약물함량，건립근홍외정량모형，용우하간중광알약물쾌속무손검측。모형채용편최소이승법（PLS）의합，광알밀정화광알이갑기밀정적정표모형상관계수분별체0.98화0.94이상。모형적표준편차（RMSECV）<6%，표명해모형능준학쾌속지측정하간중적광알밀정화광알이갑기밀정함량，차가용우실제생산중。
In order to achieve rapid nondestructive determination of sulfadiazine and sulfamethazine contents in dried shirimp,near-infrared quantitative models were established by fitting the near-infrared diffuse reflectance spectral data of prawn with its chemical values. The models were further developed by partial least square (PLS) regression and the correlation coefficients of the calibration models obtained were above 0.98 and 0.94 , respectively, which gave more reliable prediction than its near-infrared transmission counterpart. The RMSECV values were both less than 6%, showing excellent effectiveness of the models developed in this study in predicting SAs contents in dried prown.
