CAJ | 학술논문

目的：测定和分析山茱萸及其不同炮制品中马钱苷、莫诺苷、5-羟甲基糠醛、没食子酸、多糖、总黄酮、水溶性皂苷和有机酸的含量，评价炮制对山茱萸效应物质的影响。方法采用高效液相色谱法测定山茱萸不同饮片中马钱苷、莫诺苷、5-羟甲基糠醛和没食子酸的含量，采用比色法测定山茱萸不同饮片中多糖、总黄酮和水溶性皂苷的含量，采用酸碱滴定法测定山茱萸不同饮片中有机酸的含量。结果山茱萸经炮制后所测成分的含量都有不同程度的变化，除莫诺苷外，高压蒸制品所测成分的含量均略高于常压蒸制品，但均无显著性差异。结论高压蒸制工艺优于常压蒸制工艺，测定结果可为制定山茱萸最佳炮制工艺提供科学的依据。
목적：측정화분석산수유급기불동포제품중마전감、막낙감、5-간갑기강철、몰식자산、다당、총황동、수용성조감화유궤산적함량，평개포제대산수유효응물질적영향。방법채용고효액상색보법측정산수유불동음편중마전감、막낙감、5-간갑기강철화몰식자산적함량，채용비색법측정산수유불동음편중다당、총황동화수용성조감적함량，채용산감적정법측정산수유불동음편중유궤산적함량。결과산수유경포제후소측성분적함량도유불동정도적변화，제막낙감외，고압증제품소측성분적함량균략고우상압증제품，단균무현저성차이。결론고압증제공예우우상압증제공예，측정결과가위제정산수유최가포제공예제공과학적의거。
ObjectiveTo determine and analyze the contents of loginan, morroniside, 5-hydroxymethyl furfural, gallic acid, polysaccharide, lfavonooids, water-soluble saponins and organic acid in cornus ofifcinalis and its different processed products to evaluate the inlfuence of processed on active substances in cornus ofifcinalis.MethodsThe contents of loginan, morroniside, 5-Hydroxymethyl furfural and gallic acid in different processed products of cornus officinalis were determined by HPLC. The contents of polysaccharide, flavonooids, water-soluble saponins in different processed products of cornus ofifcinalis were determined by colorimetry. The contents of organic acid in different processed products of cornus ofifcinalis were determined by acid-base titration.ResultsThere were different changes of the components in cornus ofifcinalis processed by different methods. The contents of the determined components in high-pressure products of Cornus ofifcinalis were slightly higher than them in atmospheric-pressure products of cornus ofifcinalis except morroniside, but there were not signiifcant difference.ConculusionThe high-pressure process is better than the atmospheric-pressure process. The results can provide a scientiifc basis for the best processing technology of cornus ofifcinalis.