浙江化工
浙江化工
절강화공
ZHEJIANG CHEMICAL INDUSTRY
2014年
7期
27-29
,共3页
刘瑶%苏露%田香梅%赵丹%岳思雨%卢久富
劉瑤%囌露%田香梅%趙丹%嶽思雨%盧久富
류요%소로%전향매%조단%악사우%로구부
硼酸铜%复合物%制备%表征
硼痠銅%複閤物%製備%錶徵
붕산동%복합물%제비%표정
copper metaborate%composition%preparation%characterization
采用硼酸熔融法,以乙酸铜和硼酸为主要原料,制得了微米级的球状偏硼酸铜;采用水热法,以硝酸铜和硼酸为主要原料,合成了微米级的氧化亚铜和溴化亚铜复合物。通过X射线粉晶衍射(XRD)、扫描电子显微镜(SEM)等手段对合成产物进行了物相鉴定及形貌分析。
採用硼痠鎔融法,以乙痠銅和硼痠為主要原料,製得瞭微米級的毬狀偏硼痠銅;採用水熱法,以硝痠銅和硼痠為主要原料,閤成瞭微米級的氧化亞銅和溴化亞銅複閤物。通過X射線粉晶衍射(XRD)、掃描電子顯微鏡(SEM)等手段對閤成產物進行瞭物相鑒定及形貌分析。
채용붕산용융법,이을산동화붕산위주요원료,제득료미미급적구상편붕산동;채용수열법,이초산동화붕산위주요원료,합성료미미급적양화아동화추화아동복합물。통과X사선분정연사(XRD)、소묘전자현미경(SEM)등수단대합성산물진행료물상감정급형모분석。
Ball-like micron copper metaborate was obtained by Boric acid flux synthesis method, using copper acetate and boric acid as the main raw materials. In addition, micron Cu2O-CuBr composition was ob-tained by hydrothermal synthesis method, using copper nitrate and boric acid as the main raw materials. All the products were characterized by X ray powder diffraction (XRD) and scanning electron microscopy(SEM).