中国土壤与肥料
中國土壤與肥料
중국토양여비료
SOIL AND FERTILIZER SCIENCES IN CHINA
2014年
4期
97-101
,共5页
李桂花%叶小兰%杨森%温云杰%黄金生%刘云霞%汪洪
李桂花%葉小蘭%楊森%溫雲傑%黃金生%劉雲霞%汪洪
리계화%협소란%양삼%온운걸%황금생%류운하%왕홍
土壤总碳%测定方法%催化氧化法%直接燃烧法
土壤總碳%測定方法%催化氧化法%直接燃燒法
토양총탄%측정방법%최화양화법%직접연소법
soil total carbon%determination method%catalytic oxidation%direct combustion
土壤碳库由有机碳库和无机碳库两大部分组成。选择黑土和潮土两种不同类型土壤,分别通过直接燃烧和催化氧化方法测定土壤总碳含量,以揭示两种方法测定结果的可比性及其差导显著性,每个样品每种方法重复测定5次。结果表明:催化氧化法和直接燃烧法测定的黑土总碳含量平均值分别为(15.10±0.03) g/kg 和(15.38±0.32) g/kg, t检验两种方法的测定结果无明显差异。催化氧化法测定的潮土总碳含量为(15.07±0.06) g/kg,直接燃烧法测定潮土总碳含量为(15.76±0.18) g/kg, t检验结果差异明显。两种仪器土壤总碳测定结果精密度均较高,相对偏差均小于5%。为采用仪器方法测定土壤总碳含量及土壤碳库量变化提供参考。
土壤碳庫由有機碳庫和無機碳庫兩大部分組成。選擇黑土和潮土兩種不同類型土壤,分彆通過直接燃燒和催化氧化方法測定土壤總碳含量,以揭示兩種方法測定結果的可比性及其差導顯著性,每箇樣品每種方法重複測定5次。結果錶明:催化氧化法和直接燃燒法測定的黑土總碳含量平均值分彆為(15.10±0.03) g/kg 和(15.38±0.32) g/kg, t檢驗兩種方法的測定結果無明顯差異。催化氧化法測定的潮土總碳含量為(15.07±0.06) g/kg,直接燃燒法測定潮土總碳含量為(15.76±0.18) g/kg, t檢驗結果差異明顯。兩種儀器土壤總碳測定結果精密度均較高,相對偏差均小于5%。為採用儀器方法測定土壤總碳含量及土壤碳庫量變化提供參攷。
토양탄고유유궤탄고화무궤탄고량대부분조성。선택흑토화조토량충불동류형토양,분별통과직접연소화최화양화방법측정토양총탄함량,이게시량충방법측정결과적가비성급기차도현저성,매개양품매충방법중복측정5차。결과표명:최화양화법화직접연소법측정적흑토총탄함량평균치분별위(15.10±0.03) g/kg 화(15.38±0.32) g/kg, t검험량충방법적측정결과무명현차이。최화양화법측정적조토총탄함량위(15.07±0.06) g/kg,직접연소법측정조토총탄함량위(15.76±0.18) g/kg, t검험결과차이명현。량충의기토양총탄측정결과정밀도균교고,상대편차균소우5%。위채용의기방법측정토양총탄함량급토양탄고량변화제공삼고。
Soil Carbon ( C) exists in both organic and inorganic forms. We compared the results of soil C values obtained by direct combustion method and catalytic combustions method. The black soil from Heilongjiang province in Northeast China and the calcareous fluvo-aquic soil from Shandong province in North China Plain were selected. The results showed that the C con-tents of black soil samples measured by the catalytic oxidation and the direct combustion method were (15. 10 ± 0. 03) g/kg and (15. 38 ± 0. 32) g/kg, respectively, with no significant difference according to t test. The C contents of fluvo-aquic soil samples were (15. 07 ± 0. 06) g /kg through catalytic oxidation method and (15. 76 ± 0. 18) g /kg by the direct com-bustion method and presented significant difference by t test. Both methods for soil C measurement had a high precision with relative standard deviation ( RSD) less than 5%. Compared with the catalytic oxidation method, the direct combustion meas-urement showed slightly higher levels of the standard deviation and the measurement uncertainty.