CAJ | 학술논문

以SDE法提取小黄菊鲜花和制成品的香精油，用GC-MS进行定性定量分析，发现：（1）从鲜花和制成品中分别检出76和88种化合物，主要成分是单萜、倍半萜及含氧衍生物；（2）鲜花和制成品中共有成分62种，其中含量较高的有桉叶醇、樟脑、马鞭草烯醇乙酸酯、六甲基苯等；（3）在鲜花中的含量至少十倍于制成品的组分有莰烯、β-水芹烯、α-水芹烯、（E）-罗勒烯、（Z）-罗勒烯、二环[2.2.2]辛-5-烯-2-酮、别罗勒烯、D-马鞭草烯酮、藏花醛、六甲基苯；（4）鲜花精油中有14种组分是制成品精油中没有的，有α-宁烯醛、α-小茴香烯、古巴烯等；（5）制成品精油中的含量远高于鲜花中含量的组分有6-甲基-5-庚烯-2-酮、α-姜烯、β-倍半水芹烯、α-柠檬醛、棕榈酸、α-姜黄烯、反-柠檬烯氧化物、α-没药醇等；（6）制成品中特有组分有26种，有麝香草酚、苯乙醛、α-萜品醇、γ-毕澄茄烯等。研究结果揭示了小黄菊香气特征，可供栽培、加工和品审时参考。
이SDE법제취소황국선화화제성품적향정유，용GC-MS진행정성정량분석，발현：（1）종선화화제성품중분별검출76화88충화합물，주요성분시단첩、배반첩급함양연생물；（2）선화화제성품중공유성분62충，기중함량교고적유안협순、장뇌、마편초희순을산지、륙갑기분등；（3）재선화중적함량지소십배우제성품적조분유감희、β-수근희、α-수근희、（E）-라륵희、（Z）-라륵희、이배[2.2.2]신-5-희-2-동、별라륵희、D-마편초희동、장화철、륙갑기분；（4）선화정유중유14충조분시제성품정유중몰유적，유α-저희철、α-소회향희、고파희등；（5）제성품정유중적함량원고우선화중함량적조분유6-갑기-5-경희-2-동、α-강희、β-배반수근희、α-저몽철、종려산、α-강황희、반-저몽희양화물、α-몰약순등；（6）제성품중특유조분유26충，유사향초분、분을철、α-첩품순、γ-필징가희등。연구결과게시료소황국향기특정，가공재배、가공화품심시삼고。
The essential oils of fresh flowers and manufactured goods of Chrysanthemum cultivar Dendrathema grandiflorum‘Xiao Huang'Ju were extracted by the simultaneous distillation extraction method , then detected by gas chromatography coupled of mass spectrum .The results were as follows:(1) Seventy-six and eighty-eight components were respectively identified from the fresh flowers and manufactured goods of ‘Xiao Huang'Ju, with monterpenes , sesquiterpenes and their oxygenous derivatives being the major chemical components ;(2) Sixty-two mutual chemical components were identified , with eucalyptol , camphor , verbenol acetate , hexamethyl-benzene and so on at high content level.(3) The compounds in essential oils of the fresh flowers which were at least ten times greater than those in essential oils of manufactured goods were camphene ,β-phellandrene,α-phellandrene, (E)-ocimene, (Z)-ocimene, bicyclo[2.2.2]oct-5-en-2-one, allo-ocimene, D-verbenone, safranal, hexamethyl-benzene;(4) Fourteen components were only identified from the essential oils of fresh flowers , such asα-thujenal ,α-fenchene , copaene and so on.(5) The relative contents of 6-methyl-5-hepten-2-one, α-zingiberene, β-sesquiphellandrene, α-citral, palmitic acid,α-curcumene, (E)-limonene oxide,α-bisabol and so on in essential oils of manufactured goods were much more than those of fresh flower . ( 6 ) Twenty-six specific components were only identified from the manufactured goods, including thymol, benzeneacetaldehyde, α-terpineol, γ-cadinene and so on.The results revealed the chemical characteristics of aroma of ‘Xiao Huang'Ju, which can be used as the reference during its cultivating, processing and tasting .