应用化工
應用化工
응용화공
APPLIED CHEMICAL INDUSTRY
2014年
8期
1416-1418
,共3页
朱良俊%崔玉民%苗慧%尹虎%陶栋梁
硃良俊%崔玉民%苗慧%尹虎%陶棟樑
주량준%최옥민%묘혜%윤호%도동량
纳米氧化锌%光催化%甲基橙
納米氧化鋅%光催化%甲基橙
납미양화자%광최화%갑기등
nano-ZnO%photocatalysis%methyl orange
以硝酸锌、聚乙烯吡咯烷酮为原料,反应温度为80℃,反应时间为8 h,通过加热煅烧制备出纳米氧化锌粉体,煅烧温度500℃可制备纳米级的 ZnO 粉末,平均粒径为32 nm;水溶液中甲基橙在ZnO光照催化下,能迅速分解。以甲基橙为脱色对象,讨论了催化剂用量、光照时间及pH值对光催化降解甲基橙性能的影响。
以硝痠鋅、聚乙烯吡咯烷酮為原料,反應溫度為80℃,反應時間為8 h,通過加熱煅燒製備齣納米氧化鋅粉體,煅燒溫度500℃可製備納米級的 ZnO 粉末,平均粒徑為32 nm;水溶液中甲基橙在ZnO光照催化下,能迅速分解。以甲基橙為脫色對象,討論瞭催化劑用量、光照時間及pH值對光催化降解甲基橙性能的影響。
이초산자、취을희필각완동위원료,반응온도위80℃,반응시간위8 h,통과가열단소제비출납미양화자분체,단소온도500℃가제비납미급적 ZnO 분말,평균립경위32 nm;수용액중갑기등재ZnO광조최화하,능신속분해。이갑기등위탈색대상,토론료최화제용량、광조시간급pH치대광최화강해갑기등성능적영향。
Using Zn(NO3)2·6H2O and(C6H9NO)n as raw materials,the reaction temperature at 80 ℃and reaction time for 8 h,nano-ZnO powder was prepared by the method of calcining co-precipitation at 500 ℃. The average radius of nano ZnO was 32 nm. Under the UV light,methyl orange in aqueous solu-tion can quickly be decomposed by ZnO catalyst. The effects of amount of catalyst,light time and pH val-ue on photocatalytic degradation of methyl orange were discussed.