云南化工
雲南化工
운남화공
YUNNAN CHEMICAL TECHNOLOGY
2014年
4期
29-33
,共5页
熊宝林%姚莎%邱小梅%王蕾
熊寶林%姚莎%邱小梅%王蕾
웅보림%요사%구소매%왕뢰
挥发性有机物%挥发性卤代烃%室内空气质量
揮髮性有機物%揮髮性滷代烴%室內空氣質量
휘발성유궤물%휘발성서대경%실내공기질량
Volatile Organic Compounds (VOCs)%Volatile Halohydrocarbons (VHCs)%Indoor Air Quality (IAQ)%sorbent adsorption/thermal desorption%Carbon Molecular Sieve (CMS)
根据吸附剂对挥发性有机物(VOCs)的吸附原理,结合吹扫捕集仪自行研制了 VOCs气体采样管,利用 VOCs 气体采样管结合吹扫捕集仪与气相色谱仪联用,建立了完整的大气中 VOCs的分析方法,并应用于空气中挥发性卤代烃(VHCs)的检测。结果表明,VOCs 气体采样管对 VHCs 具有很好的吸附解吸效率,分析方法检出限为0.02~0.1μg/m3(进样量1L),RSD 在3.7%~8.7%之间,回收率92.4%~98.2%,满足痕量物质分析要求。
根據吸附劑對揮髮性有機物(VOCs)的吸附原理,結閤吹掃捕集儀自行研製瞭 VOCs氣體採樣管,利用 VOCs 氣體採樣管結閤吹掃捕集儀與氣相色譜儀聯用,建立瞭完整的大氣中 VOCs的分析方法,併應用于空氣中揮髮性滷代烴(VHCs)的檢測。結果錶明,VOCs 氣體採樣管對 VHCs 具有很好的吸附解吸效率,分析方法檢齣限為0.02~0.1μg/m3(進樣量1L),RSD 在3.7%~8.7%之間,迴收率92.4%~98.2%,滿足痕量物質分析要求。
근거흡부제대휘발성유궤물(VOCs)적흡부원리,결합취소포집의자행연제료 VOCs기체채양관,이용 VOCs 기체채양관결합취소포집의여기상색보의련용,건립료완정적대기중 VOCs적분석방법,병응용우공기중휘발성서대경(VHCs)적검측。결과표명,VOCs 기체채양관대 VHCs 구유흔호적흡부해흡효솔,분석방법검출한위0.02~0.1μg/m3(진양량1L),RSD 재3.7%~8.7%지간,회수솔92.4%~98.2%,만족흔량물질분석요구。
Based on the principles of Volatile Organic Compounds (VOCs)adsorption on various sorbents,an air sample tube matching up to the Purge and Trap Concentrator for VOCs was developed.Cou-pled with Purge and Trap Concentrator and gas chromatography (GC),a comprehensive method to determi-nate the VOCs in ambient air was established.The results of all experiments indicated that the method was a-vailable for trace organic matter analysis,the method detection limits (MDL)of this method is up to 0.02 -0.1μg/m3 (when the sample volume is 1L)and average recoveries for the target analytes were in the range of 92.4% -98.2%.The method also showed good linearity (R2 >0.99)and precision (<9%)values.