失效分析与预防
失效分析與預防
실효분석여예방
FAILURE ANALYSIS AND PREVENTION
2014年
4期
209-212
,共4页
孟江燕%范金娟%王云英%向东东%王琢
孟江燕%範金娟%王雲英%嚮東東%王琢
맹강연%범금연%왕운영%향동동%왕탁
航空有机玻璃%氙弧灯照射%相对分子质量%表面形貌%凝胶渗透色谱
航空有機玻璃%氙弧燈照射%相對分子質量%錶麵形貌%凝膠滲透色譜
항공유궤파리%선호등조사%상대분자질량%표면형모%응효삼투색보
aviation perspex%xenon arc lamp irradiation%relative molecular mass%surface morphology%gel permeation chromatiograph ( GPC)
在氙弧灯耐气候试验箱中对YB-2航空透明材料(有机玻璃)进行了1620 h的照射试验,采用凝胶渗透色谱仪(GPC)、红外光谱仪(FTIR)、差示扫描量热仪(DSC)、光电雾度仪、扫描电镜(SEM)、万能试验机表征和测试了照射不同时间有机玻璃的相对分子质量、红外吸收光谱、玻璃化温度( Tg)、透光率、表面形貌、拉伸强度等,分析氙弧灯照射对有机玻璃性能的影响。研究结果表明:在氙弧灯照射360 h后,有机玻璃的透光率和玻璃化温度未发生明显变化,也未产生新的化学基团,但相对分子质量有所下降;照射720 h后,有机玻璃的拉伸强度下降,且随照射时间的延长,拉伸强度下降越明显;照射1620 h后,有机玻璃表面出现了裂纹,拉伸强度降低了33%,即出现了老化特征。
在氙弧燈耐氣候試驗箱中對YB-2航空透明材料(有機玻璃)進行瞭1620 h的照射試驗,採用凝膠滲透色譜儀(GPC)、紅外光譜儀(FTIR)、差示掃描量熱儀(DSC)、光電霧度儀、掃描電鏡(SEM)、萬能試驗機錶徵和測試瞭照射不同時間有機玻璃的相對分子質量、紅外吸收光譜、玻璃化溫度( Tg)、透光率、錶麵形貌、拉伸彊度等,分析氙弧燈照射對有機玻璃性能的影響。研究結果錶明:在氙弧燈照射360 h後,有機玻璃的透光率和玻璃化溫度未髮生明顯變化,也未產生新的化學基糰,但相對分子質量有所下降;照射720 h後,有機玻璃的拉伸彊度下降,且隨照射時間的延長,拉伸彊度下降越明顯;照射1620 h後,有機玻璃錶麵齣現瞭裂紋,拉伸彊度降低瞭33%,即齣現瞭老化特徵。
재선호등내기후시험상중대YB-2항공투명재료(유궤파리)진행료1620 h적조사시험,채용응효삼투색보의(GPC)、홍외광보의(FTIR)、차시소묘량열의(DSC)、광전무도의、소묘전경(SEM)、만능시험궤표정화측시료조사불동시간유궤파리적상대분자질량、홍외흡수광보、파리화온도( Tg)、투광솔、표면형모、랍신강도등,분석선호등조사대유궤파리성능적영향。연구결과표명:재선호등조사360 h후,유궤파리적투광솔화파리화온도미발생명현변화,야미산생신적화학기단,단상대분자질량유소하강;조사720 h후,유궤파리적랍신강도하강,차수조사시간적연장,랍신강도하강월명현;조사1620 h후,유궤파리표면출현료렬문,랍신강도강저료33%,즉출현료노화특정。
Aviation perspex YB-2 ( PMMA) is irradiated in a xenon arc lamp weather resistance test chamber for 1 620 hours. The relative molecular mass, infrared absorption spectrum, glass transition temperature Tg, light transmittance, surface morphology and tensile strength of YB-2 PMMA exposed in xenon lamp for different durations are tested and characterized using gel permeation chromatograph ( GPC ) , infrared spectrometer ( IR ) , differential scanning calorimetry ( DSC ) , optical haze instrument, scanning electronic microscopy ( SEM ) and universal testing machine, and so as to comprehensively analyze the influence of xenon arc lamp on the performance of aviation perspex. The results showed that xenon arc lamp irradiation of 360 hours, the transmittance and glass transition temperature of the PMMA do not change significantly, and no new chemical group is produced according to the infrared testing results, but the relative molecular mass is descend, the tensile strength is decreasing after exposure of 720 hours. The surface of PMMA occured some tiny cracks and the tensile strength is descended 33%.