失效分析与预防
失效分析與預防
실효분석여예방
FAILURE ANALYSIS AND PREVENTION
2014年
4期
198-203
,共6页
刘佳%赵文侠%曲士昱%刘普%周静怡
劉佳%趙文俠%麯士昱%劉普%週靜怡
류가%조문협%곡사욱%류보%주정이
镍基高温合金%铸锭%偏析%β-NiAl%过载断裂
鎳基高溫閤金%鑄錠%偏析%β-NiAl%過載斷裂
얼기고온합금%주정%편석%β-NiAl%과재단렬
Ni-based superalloy%casting ingot%segregation%β-NiAl%overload fracture
发动机涡轮增压器用镍基铸造高温合金K418C铸锭经快速感应重熔浇铸零件时发生开裂。运用光学显微镜、扫描电子显微镜( SEM)、电子探针微束分析仪( EPMA)和透射电子显微镜( TEM)对断裂铸锭表面进行了宏观形貌及显微组织分析,并对断裂原因进行探讨。结果表明:断口附近的显微组织异常,黑色块状析出相分布于基体上,伴有穿晶裂纹,电子衍射分析表明黑色块状组织为β-NiAl,铸锭局部Al偏高使得铸锭在凝固时析出脆性相,再次快速加热产生的热应力使得裂纹在β-NiAl相与基体之间萌生并快速扩展贯穿整个铸锭,导致瞬间断裂。
髮動機渦輪增壓器用鎳基鑄造高溫閤金K418C鑄錠經快速感應重鎔澆鑄零件時髮生開裂。運用光學顯微鏡、掃描電子顯微鏡( SEM)、電子探針微束分析儀( EPMA)和透射電子顯微鏡( TEM)對斷裂鑄錠錶麵進行瞭宏觀形貌及顯微組織分析,併對斷裂原因進行探討。結果錶明:斷口附近的顯微組織異常,黑色塊狀析齣相分佈于基體上,伴有穿晶裂紋,電子衍射分析錶明黑色塊狀組織為β-NiAl,鑄錠跼部Al偏高使得鑄錠在凝固時析齣脆性相,再次快速加熱產生的熱應力使得裂紋在β-NiAl相與基體之間萌生併快速擴展貫穿整箇鑄錠,導緻瞬間斷裂。
발동궤와륜증압기용얼기주조고온합금K418C주정경쾌속감응중용요주령건시발생개렬。운용광학현미경、소묘전자현미경( SEM)、전자탐침미속분석의( EPMA)화투사전자현미경( TEM)대단렬주정표면진행료굉관형모급현미조직분석,병대단렬원인진행탐토。결과표명:단구부근적현미조직이상,흑색괴상석출상분포우기체상,반유천정렬문,전자연사분석표명흑색괴상조직위β-NiAl,주정국부Al편고사득주정재응고시석출취성상,재차쾌속가열산생적열응력사득렬문재β-NiAl상여기체지간맹생병쾌속확전관천정개주정,도치순간단렬。
K418C Ni-based superalloy casting ingots for engine turbochargers fractured during casting. Macrostructure and microstructure were studied by optical microscopy, scanning electrical microscopy ( SEM ) , electrical probe micro-analysis ( EPMA) and transmission electron microscopy ( TEM) , and the fracture mechanism was discussed. The results show that there were an amount of abnormal black phases near the fracture of K418C casting ingot, which distributed on the matrix, companied with transgranular crack. The electron diffraction result indicated that the black phase is β-NiAl, which is brittle and resulted from local segregation of Al during solidification. The cracks between β-NiAl and matrix were induced by heat stress during rapid heating and propagated rapidly across the whole ingot. Finally, the casting ingot fractured instantly.