CAJ | 학술논문

本文以4,4′-二甲氧基二苯甲酮、苯乙酮和呋喃甲醛为原料,采用新的路线,6步反应合成了一种新型萘并吡喃类化合物,借助核磁共振、质谱等检测手段对最终产物的结构进行了结构表征,并对其反应条件进行优化,提高了反应收率,最后应用紫外-可见吸收光谱对目标产物在不同溶剂中的光致变色性质进行了初步探索研究。
본문이4,4′-이갑양기이분갑동、분을동화부남갑철위원료,채용신적로선,6보반응합성료일충신형내병필남류화합물,차조핵자공진、질보등검측수단대최종산물적결구진행료결구표정,병대기반응조건진행우화,제고료반응수솔,최후응용자외-가견흡수광보대목표산물재불동용제중적광치변색성질진행료초보탐색연구。
A naphthopyran compound was synthesized by bis(4-methoxyphenyl)methanone,acetophenone and furfural through a no-vel synthesis method in 6 steps. The structure of target product was characterized by 1 H NMR and MS. The reaction conditions were optimized to improve the yields. The different photochromic behaviors of the compound in different solvents were studied by UV-Vis spectra.