山东农业大学学报(自然科学版)
山東農業大學學報(自然科學版)
산동농업대학학보(자연과학판)
JOURNAL OF SHANDONG AGRICULTURAL UNIVERSITY(NATURAL SCIENCE)
2014年
3期
418-422
,共5页
戴炳业%张民%王硕
戴炳業%張民%王碩
대병업%장민%왕석
希夫碱壳聚糖%酰基化多壁碳纳米管%吸附剂%表征
希伕堿殼聚糖%酰基化多壁碳納米管%吸附劑%錶徵
희부감각취당%선기화다벽탄납미관%흡부제%표정
Schiff base chitosan%acylchloride modified multi-walled carbon nanotubes%adsorbent%characterization
采用壳聚糖衍生物希夫碱壳聚糖和酰基化多壁碳纳米管制备了一种新型固相萃取材料--希夫碱壳聚糖-碳纳米管功能材料。利用傅里叶红外光谱仪、高分辨率透射电镜和热重分析仪分别研究了功能材料的结构、形貌特征和热性能。结果表明,希夫碱壳聚糖成功接枝到了酰基化多壁碳纳米管表面且接枝量为67%,S-CS-MWCNTs制备成功。
採用殼聚糖衍生物希伕堿殼聚糖和酰基化多壁碳納米管製備瞭一種新型固相萃取材料--希伕堿殼聚糖-碳納米管功能材料。利用傅裏葉紅外光譜儀、高分辨率透射電鏡和熱重分析儀分彆研究瞭功能材料的結構、形貌特徵和熱性能。結果錶明,希伕堿殼聚糖成功接枝到瞭酰基化多壁碳納米管錶麵且接枝量為67%,S-CS-MWCNTs製備成功。
채용각취당연생물희부감각취당화선기화다벽탄납미관제비료일충신형고상췌취재료--희부감각취당-탄납미관공능재료。이용부리협홍외광보의、고분변솔투사전경화열중분석의분별연구료공능재료적결구、형모특정화열성능。결과표명,희부감각취당성공접지도료선기화다벽탄납미관표면차접지량위67%,S-CS-MWCNTs제비성공。
The functional material of schiff base chitosan grafted MWCNTs was prepared by schiff base chitosan and the acylchloride modified MWCNTs. The structure, morphology and thermal property were characterized by FT-IR spectra, thermogravimetry and high resolution transmission electron microscopy. Results indicated that schiff base chitosan was successfully grafted onto the surface of the acylchloride modified MWCNTs and the percentage was 67%, indicating that the S-CS-MWCNTs was successfully synthesized.