贵州农业科学
貴州農業科學
귀주농업과학
GUIZHOU AGRICULTURAL SCIENCES
2014年
9期
55-58
,共4页
李玮%邵进明%雷战霞%王道平%敖茂宏%张永萍
李瑋%邵進明%雷戰霞%王道平%敖茂宏%張永萍
리위%소진명%뢰전하%왕도평%오무굉%장영평
流苏石斛%束花石斛%挥发油%气相-质谱联用法%兴义%贵州
流囌石斛%束花石斛%揮髮油%氣相-質譜聯用法%興義%貴州
류소석곡%속화석곡%휘발유%기상-질보련용법%흥의%귀주
Dendrobium fimbriatum%Dendrobium chrysanthum%volatile oil%GC-MS%Xingyi%Guizhou
为探明黔产流苏石斛茎与束花石斛茎中的挥发油组成及差异,采用固相微萃取技术分别提取贵州兴义野生流苏石斛茎与束花石斛茎中的挥发油,GC-MS法对其化学成分进行分析鉴定和计算相对百分含量。结果表明:从黔产流苏石斛茎与束花石斛茎中分离鉴定出化学成分62个和54个,其相对含量占挥发油总量的97.66%和96.65%;两者具有相同的挥发性化学成分40个,其主要成分均含有β-波旁烯、δ-杜松烯、反-2-辛烯醛等;其中,流苏石斛茎挥发油中相对含量最高的为β-波旁烯(47.53%),而束花石斛中相对含量最高的为依兰油烯(19.397%)。
為探明黔產流囌石斛莖與束花石斛莖中的揮髮油組成及差異,採用固相微萃取技術分彆提取貴州興義野生流囌石斛莖與束花石斛莖中的揮髮油,GC-MS法對其化學成分進行分析鑒定和計算相對百分含量。結果錶明:從黔產流囌石斛莖與束花石斛莖中分離鑒定齣化學成分62箇和54箇,其相對含量佔揮髮油總量的97.66%和96.65%;兩者具有相同的揮髮性化學成分40箇,其主要成分均含有β-波徬烯、δ-杜鬆烯、反-2-辛烯醛等;其中,流囌石斛莖揮髮油中相對含量最高的為β-波徬烯(47.53%),而束花石斛中相對含量最高的為依蘭油烯(19.397%)。
위탐명검산류소석곡경여속화석곡경중적휘발유조성급차이,채용고상미췌취기술분별제취귀주흥의야생류소석곡경여속화석곡경중적휘발유,GC-MS법대기화학성분진행분석감정화계산상대백분함량。결과표명:종검산류소석곡경여속화석곡경중분리감정출화학성분62개화54개,기상대함량점휘발유총량적97.66%화96.65%;량자구유상동적휘발성화학성분40개,기주요성분균함유β-파방희、δ-두송희、반-2-신희철등;기중,류소석곡경휘발유중상대함량최고적위β-파방희(47.53%),이속화석곡중상대함량최고적위의란유희(19.397%)。
The chemical components and relative percentage composition of volatile oil of wild D. fimbriatum and D.chrysanthum collected from Xingyi,Guizhou were analyzed and calculated by solid phase microextraction (SPME)and GC-MS to study composition and difference of volatile oil between D. fimbriatum and D.chrysanthum.The results showed that 62 and 54 chemical components are isolated and identified from D.fimbriatum and D.chrysanthum respectively,and the relative content accounts for 97.66% and 96.65% of total volatile oil amount separately.D.fimbriatum and D.chrysanthum both have the same 40 volatility chemical components,and main components areβ-bourbonene,δ-cadinene and (E)-2-octenal,etc.Theβ-bourbonene content of D.fimbriatum is the highest (47.53%)while muurdene content of D.chrysanthum is the highest (1 9 .3 9 7%).