广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2014年
16期
95-96
,共2页
气相色谱法%二硫化碳%一氯乙烷
氣相色譜法%二硫化碳%一氯乙烷
기상색보법%이류화탄%일록을완
gas chromatography%carbon disulfide%monochloro ethane
建立了活性炭吸附,二硫化碳解吸,用NNOWAX毛细管柱分离,氢火焰离子化检测器检测,时间定性,峰面积定量测定环境空气中一氯乙烷的方法。本方法的回收率为94.8%~104%之间,当采样体积为30 L,一氯乙烷最低检出质量浓度为0.007 mg/m3。本方法前处理简便,分离度好,分析灵敏度高,满足环境分析要求。
建立瞭活性炭吸附,二硫化碳解吸,用NNOWAX毛細管柱分離,氫火燄離子化檢測器檢測,時間定性,峰麵積定量測定環境空氣中一氯乙烷的方法。本方法的迴收率為94.8%~104%之間,噹採樣體積為30 L,一氯乙烷最低檢齣質量濃度為0.007 mg/m3。本方法前處理簡便,分離度好,分析靈敏度高,滿足環境分析要求。
건립료활성탄흡부,이류화탄해흡,용NNOWAX모세관주분리,경화염리자화검측기검측,시간정성,봉면적정량측정배경공기중일록을완적방법。본방법적회수솔위94.8%~104%지간,당채양체적위30 L,일록을완최저검출질량농도위0.007 mg/m3。본방법전처리간편,분리도호,분석령민도고,만족배경분석요구。
The adsorption of activated carbon , desorbed with carbon disulfide , separated by NNOWAX capillary column , hydrogen flame ionization detector , time qualitative , quantitative determination method of peak area of a chloride in ambient air.The recoveries of this method was 94.8%~104%, when the sampling volume was 30 L, a chloride minimum detection concentration was 0.007 mg/m3.The method was simple , good degree of separation , and high sensitivity , which met the demands of environmental analysis.