内蒙古民族大学学报(自然科学版)
內矇古民族大學學報(自然科學版)
내몽고민족대학학보(자연과학판)
JOURNAL OF INNER MONGOLIA UNIVERSITY FOR NATIONALITIES(NATURAL SCIENCES)
2014年
5期
582-584
,共3页
包晓华%赵贤芳%王秀兰%吴玉莲
包曉華%趙賢芳%王秀蘭%吳玉蓮
포효화%조현방%왕수란%오옥련
洁妇康洗剂%薄层色谱法%鉴别
潔婦康洗劑%薄層色譜法%鑒彆
길부강세제%박층색보법%감별
Jiefukang Lotion%Thin-layer chromatography%Identification
目的:建立蒙药洁妇康洗剂的薄层鉴别方法。方法:采用薄层色谱法鉴别该处方中苦参、关黄柏、栀子、诃子。结果:检出了该处方中苦参代表性化学成分苦参碱和氧化苦参碱、关黄柏的小檗碱、栀子的栀子苷和诃子的没食子酸,色谱分离好,斑点清晰,阴性对照无干扰。结论:该方法简便快捷,具有较好的专属性和重复性,可用于洁妇康洗剂质量的定性控制。
目的:建立矇藥潔婦康洗劑的薄層鑒彆方法。方法:採用薄層色譜法鑒彆該處方中苦參、關黃柏、梔子、訶子。結果:檢齣瞭該處方中苦參代錶性化學成分苦參堿和氧化苦參堿、關黃柏的小檗堿、梔子的梔子苷和訶子的沒食子痠,色譜分離好,斑點清晰,陰性對照無榦擾。結論:該方法簡便快捷,具有較好的專屬性和重複性,可用于潔婦康洗劑質量的定性控製。
목적:건립몽약길부강세제적박층감별방법。방법:채용박층색보법감별해처방중고삼、관황백、치자、가자。결과:검출료해처방중고삼대표성화학성분고삼감화양화고삼감、관황백적소벽감、치자적치자감화가자적몰식자산,색보분리호,반점청석,음성대조무간우。결론:해방법간편쾌첩,구유교호적전속성화중복성,가용우길부강세제질량적정성공제。
Objective:To establish the identification method of Jiefukang lotion. Methods:Sophorae flavescentis Ra-dix, Phellodendri amurensis Cortex, Gardeniae Fructus, Chebulae Fructus in the formula were identified by TLC. Re-sults:The characteristic spots of matrine and oxymatrine in the Sophorae flavescentis Radix, berberine in the Phello-dendri amurensis Cortex, geniposide in the Gardeniae Fructus, gallic acid in the Chebulae Fructus were detected. The TLC spots were clear and well-separated, and the negative control showed no interference. Conclusion: Since the method is simple and convenient, and has good specificity and reproducibility, it can be used as the qualitative quality control of Jiefukang cotion.