酿酒科技
釀酒科技
양주과기
LIQUOR-MAKING SCIENCE & TECHNOLOGY
2014年
9期
96-99
,共4页
白酒丢糟%碱液蒸煮%氯化锌活化%活性炭
白酒丟糟%堿液蒸煮%氯化鋅活化%活性炭
백주주조%감액증자%록화자활화%활성탄
distiller's grains%alkali boiling%zinc chloride chemical activation%active carbon
以白酒丢糟为原料制备活性炭。采用响应面分析法对NaOH溶液预处理去除丢糟蛋白的工艺参数进行优化，确定最佳预处理条件为：碱液浓度2.5 mol/L，碱煮时间2 h，固液比1：4，此时蛋白残留量为1.116%。采用Zn-Cl2活化后高温煅烧法制备活性炭，得出最佳制备条件为：ZnCl2质量浓度50%，料液比1：2，煅烧温度600℃，煅烧时间120 min。在最佳工艺条件下制得活性炭的亚甲基蓝吸附值最高可达到208 mg/g。
以白酒丟糟為原料製備活性炭。採用響應麵分析法對NaOH溶液預處理去除丟糟蛋白的工藝參數進行優化，確定最佳預處理條件為：堿液濃度2.5 mol/L，堿煮時間2 h，固液比1：4，此時蛋白殘留量為1.116%。採用Zn-Cl2活化後高溫煅燒法製備活性炭，得齣最佳製備條件為：ZnCl2質量濃度50%，料液比1：2，煅燒溫度600℃，煅燒時間120 min。在最佳工藝條件下製得活性炭的亞甲基藍吸附值最高可達到208 mg/g。
이백주주조위원료제비활성탄。채용향응면분석법대NaOH용액예처리거제주조단백적공예삼수진행우화，학정최가예처리조건위：감액농도2.5 mol/L，감자시간2 h，고액비1：4，차시단백잔류량위1.116%。채용Zn-Cl2활화후고온단소법제비활성탄，득출최가제비조건위：ZnCl2질량농도50%，료액비1：2，단소온도600℃，단소시간120 min。재최가공예조건하제득활성탄적아갑기람흡부치최고가체도208 mg/g。
In the experiments, distiller's grains were used to produce active carbon. The pretreatment conditions of distiller's grains (pretreated by sodium hydroxide solution to remove its proteins) were optimized by response surface method as follows:sodium hydroxide solution concentra-tion was 2.5 mol/L, boiling time was 2 h, and solid-liquid ratio was 1:4, as a result, the residual rate of protein was 1.116 %. Then after ZnCl2 chemical activation, high temperature calcination activation was adopted for the preparation of active carbon and the optimum technical parame-ters were summed up as follows: ZnCl2 concentration was 50%, solid-liquid ratio was 1:2, calcination time was 120 min, and calcination temper-ature was at 600℃. Under the above conditions, the methylene blue absorption value of the produced active carbon reached up to 208 mg/g.
