酿酒科技
釀酒科技
양주과기
LIQUOR-MAKING SCIENCE & TECHNOLOGY
2014年
9期
37-41
,共5页
陈仁远%冯永渝%梁桂娟%孙棣%寻思颖
陳仁遠%馮永渝%樑桂娟%孫棣%尋思穎
진인원%풍영투%량계연%손체%심사영
白酒%生产加工环节%甜味剂%方法检出限%本底值%来源
白酒%生產加工環節%甜味劑%方法檢齣限%本底值%來源
백주%생산가공배절%첨미제%방법검출한%본저치%래원
Baijiu(liquor)%processing procedures%sweetener%detection limit%background value%source
本研究重点围绕白酒生产加工环节中的产品因素、人为因素和环境因素,对企业生产工艺情况进行调查研究,同时设计科学的采样方案进行取样检测,探索识别白酒中甜味剂的本底值及可能来源路径。通过分析验证:所有正常生产过程酒及成品酒中的4种甜味剂(甜蜜素、糖精钠、安赛蜜、三氯蔗糖)的检出值均分别远低于0.1 mg/kg、1.0 mg/kg、4.0 mg/kg、4.0 mg/kg的国标现行方法检出限。仅甜蜜素可能考虑本底值存在,但超过国家标准检出限,应视为非法添加,不存在误判的问题。深入研究证明白酒中甜味剂的主要来源:在排除人为非法添加的前提下,外购基酒及外购调味酒是引入的主要渠道。同时提出管理建议供白酒生产企业和监管部门参考。
本研究重點圍繞白酒生產加工環節中的產品因素、人為因素和環境因素,對企業生產工藝情況進行調查研究,同時設計科學的採樣方案進行取樣檢測,探索識彆白酒中甜味劑的本底值及可能來源路徑。通過分析驗證:所有正常生產過程酒及成品酒中的4種甜味劑(甜蜜素、糖精鈉、安賽蜜、三氯蔗糖)的檢齣值均分彆遠低于0.1 mg/kg、1.0 mg/kg、4.0 mg/kg、4.0 mg/kg的國標現行方法檢齣限。僅甜蜜素可能攷慮本底值存在,但超過國傢標準檢齣限,應視為非法添加,不存在誤判的問題。深入研究證明白酒中甜味劑的主要來源:在排除人為非法添加的前提下,外購基酒及外購調味酒是引入的主要渠道。同時提齣管理建議供白酒生產企業和鑑管部門參攷。
본연구중점위요백주생산가공배절중적산품인소、인위인소화배경인소,대기업생산공예정황진행조사연구,동시설계과학적채양방안진행취양검측,탐색식별백주중첨미제적본저치급가능래원로경。통과분석험증:소유정상생산과정주급성품주중적4충첨미제(첨밀소、당정납、안새밀、삼록자당)적검출치균분별원저우0.1 mg/kg、1.0 mg/kg、4.0 mg/kg、4.0 mg/kg적국표현행방법검출한。부첨밀소가능고필본저치존재,단초과국가표준검출한,응시위비법첨가,불존재오판적문제。심입연구증명백주중첨미제적주요래원:재배제인위비법첨가적전제하,외구기주급외구조미주시인입적주요거도。동시제출관리건의공백주생산기업화감관부문삼고。
In this study, we made survey on product factors, manmade factors and environmental factors in liquor processing procedures and meanwhile designed a scientific sampling program for liquor detection in order to explore the background value and the source of sweeteners in liquor. Through the analysis and the validation, we found that, the detection values of four sweeteners (sodium cyclamate, sodium saccharin, ace-sulfame, sucralose) in all normally-produced base liquor and product liquor were far lower than the existed national detection limits (0.1 mg/kg, 1.0 mg/kg, 4.0 mg/kg, and 4.0 mg/kg respectively). Background value might only possibly exist in cyclamate. However, as its detection value ex-ceeded national detection limit, it might be induced by illegal addition, and there was no misjudgment here. The main source of sweeteners in liquor, except manmade illegal addition, might mainly come from the purchased base liquor and the purchased flavoring liquor. The related management advices were put forward for reference for distilleries and liquor supervision department.