香料香精化妆品
香料香精化妝品
향료향정화장품
FLAVOUR FRAGRANCE COSMETICS
2014年
4期
24-27
,共4页
奚安%石铭亮%李德国%章伟%王加兴
奚安%石銘亮%李德國%章偉%王加興
해안%석명량%리덕국%장위%왕가흥
溶剂提取%烟草净油%复合溶剂%协同作用
溶劑提取%煙草淨油%複閤溶劑%協同作用
용제제취%연초정유%복합용제%협동작용
solvent extraction%tobacco absolute%compound solvent%synergistic effect
通过环己烷、乙醇及其复合溶剂提取烟草净油工艺的研究,探讨了复合溶剂配比、液料比、浸提温度、浸提时间等因素对烟草净油收率的影响,并考察了溶剂对烟草净油致香成分的影响。净油收率随溶剂极性增强而增大;从烟草净油收率、节约溶剂和降低能耗的角度考虑,提取液料质量比选定为6∶1;考虑到烟草净油收率和热敏性物质的稳定性,最佳提取温度设定为50℃。使用混合溶剂提取可以利用不同溶剂组分的协同作用,提高有效成分的提取率,降低杂质含量,进而提高烟草净油的品质。
通過環己烷、乙醇及其複閤溶劑提取煙草淨油工藝的研究,探討瞭複閤溶劑配比、液料比、浸提溫度、浸提時間等因素對煙草淨油收率的影響,併攷察瞭溶劑對煙草淨油緻香成分的影響。淨油收率隨溶劑極性增彊而增大;從煙草淨油收率、節約溶劑和降低能耗的角度攷慮,提取液料質量比選定為6∶1;攷慮到煙草淨油收率和熱敏性物質的穩定性,最佳提取溫度設定為50℃。使用混閤溶劑提取可以利用不同溶劑組分的協同作用,提高有效成分的提取率,降低雜質含量,進而提高煙草淨油的品質。
통과배기완、을순급기복합용제제취연초정유공예적연구,탐토료복합용제배비、액료비、침제온도、침제시간등인소대연초정유수솔적영향,병고찰료용제대연초정유치향성분적영향。정유수솔수용제겁성증강이증대;종연초정유수솔、절약용제화강저능모적각도고필,제취액료질량비선정위6∶1;고필도연초정유수솔화열민성물질적은정성,최가제취온도설정위50℃。사용혼합용제제취가이이용불동용제조분적협동작용,제고유효성분적제취솔,강저잡질함량,진이제고연초정유적품질。
The effects of ratio of cyclohexane to ethanol,ratio of liquid to solid,extraction temperature and extraction time on yield of tobacco absolute were investigated. The influence of solvent on flavor ingredients in tobacco absolute was also dis-cussed. The yield of tobacco absolute increased with the polarity of solvent. The optimized ratio of liquid to solid was set at 6/1 considering the yield of tobacco absolute,solvent saving and energy reduction. The optimized temperature was 50 ℃ based on yield of product and stability of heat-sensitive materials. The yield of tobacco absolute could be improved,and content of impu-rities could be reduced by synergistic effect of compound solvent,thus,the product with improved quality could be obtained.